1,3,5-三甲氧基苯合成路线 （共 273 条）
反应条件
tert-butyl peroxide; K2CO3; maghemite Fe2O3, .gamma., maghemite in benzene under air, (t-BuO)2 2.0 equiv., K2CO3 2.0 equiv., Fe2O3 0.2 equiv.; 80 °C, 5 d;
参考文献
Yan, Guobing; Jiang, Yubo; Kuang, Chunxiang; Wang, Shuai; Liu, Haichao; Zhang, Yan; Wang, Jianbo
Chemical Communications, 2010 , vol. 46, # 18 p. 3170 - 3172
反应条件
1: boron trifluoride diethyl etherate / 20 - 100 °C 2: iodine / dimethyl sulfoxide / 4.5 h / 130 °C View Scheme
参考文献
Zhang, Ji; Liu, Man; Cui, Wei; Yang, Jian; Yang, Bo
Journal of Chemical Research, 2014 , vol. 38, # 1 p. 60 - 61
反应条件
1: phloroglucinol trimethyl ether in dichloromethane T=0°C; 0.166667 h; 2: acetyl chloride With AlCl3, aluminium chloride in dichloromethane Friedel-Crafts Acylation; 2 h;
参考文献
Zhang, Wen-Jing; Wu, Jing-Fang; Zhou, Peng-Fei; Wang, Yang; Hou, Ai-Jun
Tetrahedron, 2013 , vol. 69, # 29 p. 5850 - 5858
反应条件
scandium tris(trifluoromethanesulfonate) in acetonitrile Friedel-Crafts Acylation; 0.5 h; Inert atmosphereMicrowave irradiationHeatingGreen chemistry; Time;
参考文献
Perrier, Arnaud; Keller, Michel; Caminade, Anne-Marie; Majoral, Jean-Pierre; Ouali, Armelle
Green Chemistry, 2013 , vol. 15, # 8 p. 2075 - 2080
反应条件
1: With hydrogenchloride; zinc(II) chloride in diethyl ether T=0 - 5°C; 72 h; 2: With water in diethyl ether T=60°C; 2 h;
参考文献
Sagrera, Gabriel; Seoane, Gustavo
Synthesis, 2010 , # 16 art. no. M06509SS, p. 2776 - 2786
反应条件
sodium perchlorate; acetic acid T=70°C;
参考文献
Mathur et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 3582,3585
反应条件
1: 1.) AlCl3; 2.) H2O, conc HCl / 1.) Et2O, reflux, 1 h then r.t., overnight 2: diethyl ether View Scheme
参考文献
Chavan, Hemant V.; Bandgar, Babasaheb P.; Adsul, Laxman K.; Dhakane, Valmik D.; Bhale, Pravin S.; Thakare, Vishnu N.; Masand, Vijay
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 5 p. 1315 - 1321
参考文献
Nakazawa; Matsuura
Yakugaku Zasshi, 1954 , vol. 74, p. 1254
Chem.Abstr., 1955 , p. 14669
参考文献
Friedlaender; Schnell
Chemische Berichte, 1897 , vol. 30, p. 2153
参考文献
v. Kostanecki; Tambor
Chemische Berichte, 1899 , vol. 32, p. 2262
