1,3,5-三甲氧基苯合成路线 （共 273 条）
反应条件
Hydrolyse des Reaktionsprodukts mit Wasser;
参考文献
Houben; Fischer
Journal fuer Praktische Chemie (Leipzig), 1929 , vol. <2> 123, p. 100
Full Text Show Details
Shinoda
Yakugaku Zasshi, 1927 , p. 111
Chem. Zentralbl., 1928 , vol. 99, # I p. 333
参考文献
PIRAMAL LIFE SCIENCES LIMITED; BANDGAR, Babasaheb Pandurang; TOTRE, Jalindar Vasant
Patent: WO2011/121505 A1, 2011 ;
Location in patent: Page/Page column 42 ;
反应条件
1: phloroglucinol trimethyl ether With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-78 - 20°C; 2 h; 3: methanol Further stages;
参考文献
Tetrahedron, , vol. 68, # 24 p. 4701 - 4709
反应条件
1: With aluminium trichloride in toluene T=20°C; 15 h; 2: With water in toluene T=20°C; 2 h; Further stages.;
参考文献
Tobisu, Mamoru; Yamaguchi, Seiji; Chatani, Naoto
Organic Letters, 2007 , vol. 9, # 17 p. 3351 - 3353
反应条件
trichlorophosphate T=40 - 50°C; Vilsmeier reaction;
参考文献
Gallardo-Godoy, Alejandra; Fierro, Angelica; McLean, Thomas H.; Castillo, Mariano; Cassels, Bruce K.; Reyes-Parada, Miguel; Nichols, David E.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 7 p. 2407 - 2419
反应条件
silver trifluoromethanesulfonate in dichloromethane T=0°C; 0.25 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 78, # 7 p. 3438 - 3444
反应条件
AlCl3, aluminium chloride in chlorobenzene T=0 - 18°C; 22 h;
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 63, # 4 p. 395 - 406
反应条件
hydrogenchloride; zinc(II) chloride; benzene Reaktion des entstandenen Aldimids mit waessr. Salzsaeure;
参考文献
Herzig; Wenzel; Gehringer
Monatshefte fuer Chemie, 1903 , vol. 24, p. 866
反应条件
water 1.) CH2Cl2, 0 deg C, 0.5 h, 2.) CH2Cl2, 20 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Pindur, U.; Flo, C.
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 1563 - 1568
反应条件
diethyl ether; trichlorophosphate anschliessend Behandeln des Reaktionsprodukts mit wss. NaOH;
参考文献
Kenyon; Mason
Journal of the Chemical Society, 1952 , p. 4964,4966
