1: isopropyl bromide With iodine; magnesium in diethyl ether
T=0°C; 0.5 h; Inert atmosphere;
2: 3-phenyl-2-propenoic acid in diethyl ether
T=0°C; 3 h; Inert atmosphereReflux;
3: With hydrogenchloride in diethyl ether; water
Cooling with ice;
参考文献
Deasy, Rebecca E.; Brossat, Maude; Moody, Thomas S.; Maguire, Anita R.
Tetrahedron Asymmetry, 2011 , vol. 22, # 1 p. 47 - 61