1,3-二羟基丙酮二聚体合成路线 （共 44 条）
反应条件
acetic acid in butan-1-ol 50 h; Ambient temperature;
参考文献
Aulaskari, Paula; Ahlgren, Markku; Rouvinen, Juha; Vainiotalo, Pirjo; Pohjala, Esko; Vepsaelaeinen, Jouko
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 4 p. 1345 - 1354
反应条件
in diethylene glycol dimethyl ether
参考文献
BP Chemicals Limited
Patent: EP460831 A2, 1991 ;
反应条件
SnCl4*5H2O T=110°C; 6 h;
参考文献
Zhang, Zehui; Zhao, Zongbao
Chinese Journal of Catalysis, 2011 , vol. 32, # 1 p. 70 - 73
反应条件
triethylamine in 1,4-dioxane
参考文献
Hoechst Marion Roussel
Patent: US6087509 A1, 2000 ;
反应条件
acetic acid in water; acetonitrile T=55°C; Marckwald imidazole synthesis; 18 h; Product distribution; Further Variations:Solvents;
参考文献
Maligres, Peter E.; Waters, Marjorie S.; Weissman, Steven A.; McWilliams, J. Christopher; Lewis, Stephanie; Cowen, Jennifer; Reamer, Robert A.; Volante; Reider, Paul J.; Askin, David
Journal of Heterocyclic Chemistry, 2003 , vol. 40, # 2 p. 229 - 241
反应条件
sodium hydroxide Erwaermen des Reaktionsprodukts in wss. NaOH mit KMnO4;
参考文献
Landor; Rydon
Journal of the Chemical Society, 1955 , p. 1113,1115
反应条件
1 h; Heating / reflux;
参考文献
Eastman Kodak Company
Patent: US6348592 B1, 2002 ;
Location in patent: Page column 15 ;
反应条件
in pyridine
14 h; Ambient temperature;
参考文献
Suemune; Mizuhara; Akita; Sakai
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 8 p. 3440 - 3444
参考文献
Schreiber, Stuart L.; Sommer, Toby J.
Tetrahedron Letters, 1983 , vol. 24, # 44 p. 4781 - 4784
反应条件
1: With acetic acid in tert-butyl alcohol
T=20°C; 48 h;
2: With nitric acid; sodium nitrite in water
T=0 - 20°C; 2 h;
参考文献
Takeda Chemical Industries, Ltd.
Patent: EP1422228 A1, 2004 ;
Location in patent: Page 216 ;
EP 1422228 A1
