2-(甲氧基甲基)苯甲醇合成路线 （共 11 条）
反应条件
pyridinium chlorochromate in dichloromethane 1.5 h; Ambient temperature;
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1465 - 1473
反应条件
1: 74 percent / PCC / CH2Cl2 / 1.5 h / Ambient temperature 2: 91 percent / ethanol / 1.) 60 deg C, 3 h, 2.) room temp., 3 h, 3.) -20 deg C, overnight 3: 0.2 M NaOC2H5 / ethanol / 2 h / Ambient temperature; Irradiation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 111, # 4 p. 1465 - 1473
反应条件
1: SOBr2; pyridine; CHCl3 3: aqueous sulfuric acid View Scheme
参考文献
Journal of the Chemical Society, , p. 2819,2824
反应条件
pyridine; thionyl bromide; chloroform
参考文献
Leonardi, Amedeo; Motta, Gianni; Riva, Carlo; Poggesi, Elena
Patent: US2004/72839 A1, 2004 ;
Location in patent: Page/Page column 36-37 ;
US 20040072839 A1
反应条件
sodium hydride in tetrahydrofuran
T=20°C;
参考文献
Zheng, Qi-Huang; Liu, Xuan; Fei, Xiangshu; Wang, Ji-Quan; Ohannesian, David W.; Erickson, Leonard C.; Stone, K. Lee; Martinez, Tanya D.; Miller, Kathy D.; Hutchins, Gary D.
Journal of Labelled Compounds and Radiopharmaceuticals, 2002 , vol. 45, # 14 p. 1239 - 1252
反应条件
methanol
T=25°C; 1 h; Irradiation; Further byproducts given. Yields of byproduct given;
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2325 - 2332
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Mann; Stewart
Journal of the Chemical Society, 1954 , p. 2819,2824
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Mann; Stewart
Journal of the Chemical Society, 1954 , p. 2819,2824
反应条件
1: pyridine
2: aq.-ethanolic NaOH
3: LiAlH4; diethyl ether
View Scheme
参考文献
Mann; Stewart
Journal of the Chemical Society, 1954 , p. 2819,2824
反应条件
1: sodium methylate
2: LiAlH4; diethyl ether
View Scheme
参考文献
Mann; Stewart
Journal of the Chemical Society, 1954 , p. 2819,2824
