N-(4-碘苯基)乙酰胺合成路线 （共 72 条）
反应条件
N,N,N',N,-tetramethylethylenediamine; copper diacetate; ammonium hydrogen carbonate T=150°C; 22 h; sealed tube;
参考文献
Zhang, Guoying; Ren, Xinyi; Chen, Jianbin; Hu, Maolin; Cheng, Jiang
Organic Letters, 2011 , vol. 13, # 19 p. 5004 - 5007
反应条件
in N,N-dimethyl-formamide T=20°C; 18 h; Inert atmosphere; Product distribution / selectivity;
参考文献
Morimoto, Hiroyuki; Tsubogo, Tetsu; Litvinas, Nichole D.; Hartwig, John F.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 16 p. 3793 - 3798
反应条件
1: copper / dimethyl sulfoxide / 12 h / 60 °C / |Inert atmosphere 2: potassium carbonate / methanol; water / 2 h / 20 °C / |Inert atmosphere 3: 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate); silver nitrate / water; acetone / 1 h / 55 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Mizuta, Satoshi; Stenhagen, Ida S.R.; O'Duill, Miriam; Wolstenhulme, Jamie; Kirjavainen, Anna K.; Forsback, Sarita J.; Tredwell, Matthew; Sandford, Graham; Moore, Peter R.; Huiban, Mickael; Luthra, Sajinder K.; Passchier, Jan; Solin, Olof; Gouverneur, Veronique
Organic Letters, 2013 , vol. 15, # 11 p. 2648 - 2651
反应条件
1: [Rh(NCMe)2(cod)][BF4]; triethylamine / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere 2: 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate); BaO; silver(l) oxide / acetone / 2 h / 23 - 90 °C View Scheme
参考文献
Tang, Pingping; Ritter, Tobias
Tetrahedron, 2011 , vol. 67, # 24 p. 4449 - 4454
参考文献
Michael; Norton
Chemische Berichte, 1878 , vol. 11, p. 109
参考文献
Michael; Norton
Chemische Berichte, 1878 , vol. 11, p. 109
Full Text Show Details
Reverdin
Bulletin de la Societe Chimique de France, 1898 , vol. <3> 19, p. 143
Full Text Show Details
Brenans
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1913 , vol. 157, p. 1156,1157
Bulletin de la Societe Chimique de France, 1914 , vol. <4>15, p. 90,92
参考文献
Michael; Norton
Chemische Berichte, 1878 , vol. 11, p. 109
反应条件
1: acetic acid; bromine / 70 °C 2: hydrochloric acid; water; alcohol View Scheme
参考文献
Heisig
Journal of the American Chemical Society, 1928 , vol. 50, p. 143
反应条件
copper diacetate; palladium diacetate; 2,2,2-trimethylacetic acid in 1,2-dichloro-ethane T=110°C; 24 h; Inert atmosphereSchlenk techniqueSealed tubeGreen chemistry;
参考文献
Zhang, Li-Sheng; Chen, Kang; Chen, Guihua; Li, Bi-Jie; Luo, Shuang; Guo, Qing-Yun; Wei, Jiang-Bo; Shi, Zhang-Jie
Organic Letters, 2013 , vol. 15, # 1 p. 10 - 13
反应条件
1: P2S5 2: K3<Fe(CN)6>; aqueous NaOH View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 35, p. 779,783
