N-(4-碘苯基)乙酰胺合成路线 （共 72 条）
反应条件
dichloro bis(acetonitrile) palladium(II); tetrabutylammomium bromide; water; zinc oxide in dimethyl sulfoxide T=100°C; 30 h;
参考文献
Organic Letters, , vol. 13, # 9 p. 2184 - 2187
反应条件
N-ethyl-N,N-diisopropylamine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; tris-(o-tolyl)phosphine in 1-methyl-pyrrolidin-2-one T=20°C; Reduction; silylation; 1 h;
参考文献
Murata, Miki; Suzuki, Katsuhiro; Watanabe, Shinji; Masuda, Yuzuru
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8569 - 8571
反应条件
formic acid; tributyl-amine; tris-fac-Ir(ppy)3 in acetonitrile T=25 - 30°C; 44 h; Inert atmosphereIrradiation;
参考文献
Nguyen, John D.; D'Amato, Erica M.; Narayanam, Jagan M. R.; Stephenson, Corey R. J.
Nature Chemistry, 2012 , vol. 4, # 10 p. 854 - 859
反应条件
ammonium hydroxide; potassium phosphate; 1-(5,6,7,8-tetrahydroquinolin-8-yl)-2-methylpropan-1-one; copper(I) bromide in dimethyl sulfoxide T=25°C; 24 h; Inert atmosphereSealed tube;
参考文献
Wang, Deping; Cai, Qian; Ding, Ke
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 11-12 p. 1722 - 1726
反应条件
1: tris-(dibenzylideneacetone)dipalladium(0); Me3SnNMe2; triphenylphosphine / toluene / 8 h / Inert atmosphere; Reflux 2: tetrabutyl ammonium fluoride / dichloromethane / 5 h / 20 °C View Scheme
参考文献
Cai, Liangzhen; Yang, Dujuan; Sun, Zhonghua; Tao, Xiaochun; Cai, Lisheng; Pike, Victor W.
Chinese Journal of Chemistry, 2011 , vol. 29, # 5 p. 1059 - 1062
反应条件
in N,N-dimethyl-formamide T=140°C; 12 h;
参考文献
Suzuki, Hitomi; Abe, Hajime
Synthetic Communications, 1996 , vol. 26, # 18 p. 3413 - 3419
反应条件
1: With copper(l) iodide; potassium carbonate; sulfur in N,N-dimethyl-formamide T=90°C; 12 h; Inert atmosphere; 2: With sodium tetrahydroborate in N,N-dimethyl-formamide T=40°C; Inert atmosphereCooling with ice;
参考文献
Organic Letters, , vol. 11, # 22 p. 5250 - 5253
参考文献
Dains; Malleis; Meyers
Journal of the American Chemical Society, 1913 , vol. 35, p. 972
反应条件
copper bronze; tetra-n-butylammonium nitrate; N-methyl-2-(methylamino)ethylamine in N,N-dimethyl-formamide T=100°C;
参考文献
Saito, Shinichi; Koizumi, Yuichiro
Tetrahedron Letters, 2005 , vol. 46, # 28 p. 4715 - 4717
参考文献
Michael; Norton
Chemische Berichte, 1878 , vol. 11, p. 109
Full Text Show Details
Reverdin
Bulletin de la Societe Chimique de France, 1898 , vol. <3> 19, p. 143
Full Text Show Details
Brenans
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1913 , vol. 157, p. 1156,1157
Bulletin de la Societe Chimique de France, 1914 , vol. <4>15, p. 90,92
