2,5-二氯-2,5-二甲基己烷合成路线 （共 77 条）
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 143, p. 496
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 143, p. 496
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 143, p. 496
参考文献
Justus Liebigs Annalen der Chemie, , vol. 583, p. 93,99
反应条件
1: 75 percent / AlCl3 / CS2 / 0.5 h / Ambient temperature 2: 87 percent / aq. KOH / methanol / 0.5 h / 70 °C View Scheme
参考文献
Dawson; Hobbs; Derdzinski; Chao; Frenking; Loew; Jetten; Napoli; Williams; Sani; Wille Jr.; Schiff
Journal of Medicinal Chemistry, 1989 , vol. 32, # 7 p. 1504 - 1517
反应条件
1: AlCl3 / CH2Cl2 2: HNO3 3: 100 percent / H2 / Pd/C / ethanol View Scheme
参考文献
Myhre,P.C.; Schubert,W.M.
Journal of Organic Chemistry, 1960 , vol. 25, p. 708 - 711
反应条件
1: 81.9 percent / AlCl3 / 24 h / Heating 2: 49.9 percent / HNO3, H2SO4 / 1 h / -10 °C 3: 48 percent / hydrogen / Pd/C / ethanol 4: 86.7 percent / pyridine / benzene / Ambient temperature 5: aq. NaOH / ethanol / Ambient temperature View Scheme
参考文献
Kagechika, Hiroyuki; Kawachi, Emiko; Hashimoto, Yuichi; Himi, Toshiyuki; Shudo, Koichi
Journal of Medicinal Chemistry, 1988 , vol. 31, # 11 p. 2182 - 2192
反应条件
1: 81.9 percent / AlCl3 / 24 h / Heating 2: 49.9 percent / HNO3, H2SO4 / 1 h / -10 °C 3: 48 percent / hydrogen / Pd/C / ethanol 4: 86.7 percent / pyridine / benzene / Ambient temperature View Scheme
参考文献
Kagechika, Hiroyuki; Kawachi, Emiko; Hashimoto, Yuichi; Himi, Toshiyuki; Shudo, Koichi
Journal of Medicinal Chemistry, 1988 , vol. 31, # 11 p. 2182 - 2192
→
22306-30-51,1,4,4,5,5,8,8-八甲基-1,2,3,4,5,6,7,8-八氢蒽
反应条件
aluminium trichloride
参考文献
Roehm and Haas Co.
Patent: US2198374 , 1938 ;
Full Text Show Details
Bruson; Kroeger
Journal of the American Chemical Society, 1940 , vol. 62, p. 36,43
→
22306-30-51,1,4,4,5,5,8,8-八甲基-1,2,3,4,5,6,7,8-八氢蒽+
反应条件
aluminium trichloride in pentane 0.666667 h; Ambient temperature;
参考文献
Myhre,P.C.; Schubert,W.M.
Journal of Organic Chemistry, 1960 , vol. 25, p. 708 - 711
