1.1: 96 percent / potassium carbonate / acetone / 4 h / Heating
2.1: 93 percent / thionyl chloride / CH2Cl2 / 3 h / 0 °C
3.1: sodium hydride / dimethylformamide / 0.5 h / 20 °C
3.2: 98 percent / dimethylformamide / 3 h
View Scheme
参考文献
Lee, Jeewoo; Lee, Ju-Hyun; Kim, Su Yeon; Perry, Nicholas A.; Lewin, Nancy E.; Ayres, Jolene A.; Blumberg, Peter M.
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 6 p. 2022 - 2031