反应条件
1: diphenylphosphoranyl azide; triethylamine / 1,4-dioxane / 2 h / 105 °C / Inert atmosphere 2: trimethylsilyl trifluoromethanesulfonate / dichloromethane / -78 - 25 °C / Molecular sieve; Inert atmosphere 3: urea hydrogen peroxide addition compound / water; acetonitrile / 3 h / 25 °C / pH 8 / aq. phosphate buffer View Scheme
参考文献
Journal of Organic Chemistry, , vol. 76, # 24 p. 10099 - 10113