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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-氯苯甲醚
合成路线
（共 685 条）
623-12-1
4-氯苯甲醚
+
162101-25-9
2,6-二氟苯硼酸
→
反应条件
717101-32-1
反应条件
potassium phosphate; 2nd generation X-Phos precatalyst in tetrahydrofuran; water T=20°C; Suzuki-Miyaura cross-coupling; 0.5 h; Inert atmosphere;
参考文献
Kinzel, Tom; Zhang, Yong; Buchwald, Stephen L.
Journal of the American Chemical Society, 2010 , vol. 132, # 40 p. 14073 - 14075
623-12-1
4-氯苯甲醚
+
5720-06-9
2-甲氧基苯基硼酸
+
162101-25-9
2,6-二氟苯硼酸
→
反应条件
717101-32-1
+
49602-47-3
反应条件
potassium phosphate; 2nd generation X-Phos precatalyst in tetrahydrofuran; water T=20°C; Suzuki-Miyaura cross-coupling; 0.5 h; Inert atmosphere;
参考文献
Kinzel, Tom; Zhang, Yong; Buchwald, Stephen L.
Journal of the American Chemical Society, 2010 , vol. 132, # 40 p. 14073 - 14075
623-12-1
4-氯苯甲醚
+
768-35-4
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
49602-47-3
+
72093-48-2
反应条件
potassium phosphate; 2nd generation X-Phos precatalyst in tetrahydrofuran; water T=20°C; Suzuki-Miyaura cross-coupling; 0.5 h; Inert atmosphere;
参考文献
Kinzel, Tom; Zhang, Yong; Buchwald, Stephen L.
Journal of the American Chemical Society, 2010 , vol. 132, # 40 p. 14073 - 14075
623-12-1
4-氯苯甲醚
+
38769-92-5
→
反应条件
726-18-1
反应条件
anhydrous nickel; carbon in tetrahydrofuran Kumada reaction; 0.166667 h; Heating;
参考文献
Park, Sun Young; Kang, Min; Yie, Jae Eui; Kim, Ji Man; Lee, Ik-Mo
Tetrahedron Letters, 2005 , vol. 46, # 16 p. 2849 - 2852
623-12-1
4-氯苯甲醚
+
479486-96-9
→
反应条件
7291-00-1
反应条件
bis(tri-tert-butylphosphine)palladium(0) in toluene T=100°C; 9 h;
参考文献
Cunico, Robert F.; Maity, Bikash C.
Organic Letters, 2002 , vol. 4, # 24 p. 4357 - 4359
623-12-1
4-氯苯甲醚
+
536-74-3
→
反应条件
7380-78-1
反应条件
potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in N,N-dimethyl-formamide T=140°C; Sonogashira cross-coupling; 20 h;
参考文献
Feuerstein, Marie; Doucet, Henri; Santelli, Maurice
Tetrahedron Letters, 2004 , vol. 45, # 46 p. 8443 - 8446
623-12-1
4-氯苯甲醚
+
637-44-5
→
反应条件
7380-78-1
反应条件
[Pd((.eta.5-C5H5)Fe[(.eta.5-C5H3)C(Me)=N(C6H4-4-Me)])(.mu.-Cl)]2; potassium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in anhydrous xylene; water T=120°C; 3 h; Reagent/catalystSolventTemperature;
参考文献
Li, Xi'Ang; Yang, Fan; Wu, Yangjie
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4543 - 4550
623-12-1
4-氯苯甲醚
+
1719-19-3
→
反应条件
7380-78-1
反应条件
{(Pd{Fe(.eta.5-C5H5)(.eta.5-C5H3C(CH3)=NC6H4CH3-4)}(.mu.-Cl))2}; potassium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in acetonitrile T=110°C; 16 h; Inert atmosphere;
参考文献
Hu, Hao; Yang, Fan; Wu, Yangjie
Journal of Organic Chemistry, 2013 , vol. 78, # 20 p. 10506 - 10511
623-12-1
4-氯苯甲醚
+
2170-06-1
→
反应条件
7380-78-1
反应条件
pyrrolidine; Najera palladacycle I; 4-laurylbenzenesulfonic acid sodium salt; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in water T=130°C; Sonogashira Cross-Coupling; 0.5 h; Microwave irradiationSealed tubeGreen chemistry; chemoselective reaction;
参考文献
Buxaderas, Eduardo; Alonso, Diego A.; Najera, Carmen
European Journal of Organic Chemistry, 2013 , # 26 p. 5864 - 5870
623-12-1
4-氯苯甲醚
+
108-90-7
+
471-25-0
→
反应条件
7380-78-1
+
2132-62-9
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; palladium dichloride; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in dimethyl sulfoxide T=120°C; 24 h; Inert atmosphere;
参考文献
Li, Xiang; Yang, Fan; Wu, Yangjie
RSC Advances, 2014 , vol. 4, # 26 p. 13738 - 13741
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