1,4-二(溴甲基)苯合成路线 (共 136 条)
反应条件
hydrogen bromide; sodium bromide in chloroform; water T=5 - 15°C; Electrolysis;
参考文献
Kulangiappar; Karthik; Kulandainathan, M. Anbu
Synthetic Communications, 2009 , vol. 39, # 13 p. 2304 - 2309
反应条件
potassium in tetrahydrofuran Heating;
参考文献
Bock,H.; Kaim,W.
Chemische Berichte, 1978 , vol. 111, p. 3552 - 3572
反应条件
potassium fluoride in N,N-dimethyl-formamide T=130°C; 0.5 h;
参考文献
Wagner, Richard W.; Johnson, Thomas E.; Lindsey, Jonathan S.
Tetrahedron, 1997 , vol. 53, # 20 p. 6755 - 6790
反应条件
sodium tetrahydroborate; tri-n-butylhexadecylphosphonium bromide in dichloromethane; water T=18°C; 0 h; Product distribution;
参考文献
Rolla, Franco
Journal of Organic Chemistry, 1981 , vol. 46, # 19 p. 3909 - 3911
反应条件
samarium diiodide in tetrahydrofuran 0.166667 h; Ambient temperature; Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 8 p. 2029 - 2032
参考文献
Stephen; Short; Gladding
Journal of the Chemical Society, 1920 , vol. 117, p. 525
参考文献
Loew
Justus Liebigs Annalen der Chemie, 1885 , vol. 231, p. 363
Full Text Show Details
Wegscheider; Suida
Monatshefte fuer Chemie, 1912 , vol. 33, p. 1010
反应条件
1: lead nitrate; water
2: PCl5
View Scheme
参考文献
Wegscheider; Suida
Monatshefte fuer Chemie, 1912 , vol. 33, p. 1010
反应条件
1: piperidine With potassium carbonate in tetrahydrofuran
0.166667 h;
2: α,alpha';-dibromo-p-xylene in tetrahydrofuran
参考文献
Saif, Muhammad Jawwad; Anwar, Jamil; Munawar, Munawar Ali; Kashif, Muhammad; Asghar, Muhammad Imran
Arkivoc, 2010 , vol. 2010, # 11 p. 133 - 145
反应条件
1: 48.5 percent / 3 h / 120 °C
View Scheme
参考文献
Nudelman, Ellen; Engel, Robert
Phosphorus, Sulfur and Silicon and the Related Elements, 1996 , vol. 111, p. 162