3-(2-呋喃基)丙烯醛合成路线 (共 28 条)
反应条件
p-benozquinone in diethylene glycol dimethyl ether T=120°C; 19 h;
参考文献
Kulkarni; Mathew
Tetrahedron Letters, 1990 , vol. 31, # 31 p. 4497 - 4500
反应条件
sodium hydroxide in water T=40°C; 0.0833333 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2081 - 2083
反应条件
(S)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine; 2,3-dicyano-5,6-dichloro-p-benzoquinone in tetrahydrofuran T=20°C; 1 h;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 17 p. 3920 - 3924
反应条件
sodium hydroxide; water T=40°C;
参考文献
Chemische Berichte, , vol. 31, p. 282
反应条件
1: toluene / 4.03 h / -70 - 20 °C / |Inert atmosphere 2: water; hydrogenchloride / pH < 3 / |Inert atmosphere View Scheme
参考文献
Organic Syntheses, , vol. 89, p. 527 - 536
反应条件
α-chymotrypsin in water enthalpy changes for base (nonenzymatic) and enzymatic (α-chymotrypsin) hydrolysis; Thermodynamic data;
参考文献
Journal of the American Chemical Society, , vol. 102, # 20 p. 6318 - 6324
参考文献
Chemische Berichte, , vol. 58, p. 2562
参考文献
Zhurnal Obshchei Khimii, , vol. 29, p. 2560,2564; engl. Ausg. S. 2524, 2527
反应条件
1: 60 percent / 85percent NH2NH2*H2O / ethanol / 7 h / Heating 2: 15 percent / Pt/C, Ag/KOH View Scheme
参考文献
Mochalov, S.S.; Abdel'razek, F.M.; Surikova, T.P.; Shabarov, Yu.S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 4 p. 339 - 344
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , vol. 16, # 4 p. 455 - 460
反应条件
lithium sodium; ammonia; lithium 1.) ether 50 min 2.) -78 deg C - room temp. 55 min 3.) 10 min; Yield given. Multistep reaction;
参考文献
Hall; Farahat
Journal of Heterocyclic Chemistry, 1987 , vol. 24, # 4 p. 1205 - 1213