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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘甲苯
合成路线
（共 1421 条）
2227-57-8
3-(4-甲氧基苯基)丙酸
+
624-31-7
4-碘甲苯
→
反应条件
24785-38-4
反应条件
copper(l) iodide; potassium carbonate; triphenylphosphine in dimethyl sulfoxide T=100°C; 24 h; Inert atmosphere;
参考文献
Li, Tingyi; Sun, Peng; Yang, Hailong; Zhu, Yan; Yan, Hong; Lu, Linhua; Mao, Jincheng
Tetrahedron, 2012 , vol. 68, # 32 p. 6413 - 6419
104-92-7
4-溴苯甲醚
+
624-31-7
4-碘甲苯
+
471-25-0
丙炔酸
→
反应条件
24785-38-4
反应条件
1: 1-(iodo)-4-methylbenzene; acetylenecarboxylic acid With bis-triphenylphosphine-palladium(II) chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,4-di(diphenylphosphino)-butane in dimethyl sulfoxide T=50°C; 4 h; 2: 1-bromo-4-methoxy-benzene in dimethyl sulfoxide T=120°C; 4 h;
参考文献
Lee, Hee Joon; Park, Kyungho; Bae, Goun; Choe, Jaehoon; Song, Kwang Ho; Lee, Sunwoo
Tetrahedron Letters, 2011 , vol. 52, # 39 p. 5064 - 5067
872356-95-1
+
624-31-7
4-碘甲苯
→
反应条件
24785-38-4
反应条件
1,3-dimethyl-imidazolidin-2-one; potassium carbonate; triphenylphosphine; copper(l) chloride T=120°C; 12 h;
参考文献
Ogawa, Daisuke; Li, Jing; Suetsugu, Masato; Jiao, Jiao; Iwasaki, Masayuki; Nishihara, Yasushi
Tetrahedron Letters, 2013 , vol. 54, # 6 p. 518 - 521
624-31-7
4-碘甲苯
→
反应条件
24785-38-4
反应条件
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 8 h / 20 °C / Inert atmosphere 2: copper(l) iodide; potassium carbonate; triphenylphosphine / dimethyl sulfoxide / 24 h / 90 °C / Inert atmosphere View Scheme
参考文献
Qu, Xiaoming; Li, Tingyi; Sun, Peng; Zhu, Yan; Yang, Hailong; Mao, Jincheng
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 20 p. 6938 - 6942
624-31-7
4-碘甲苯
+
100-61-8
N-甲基苯胺
→
反应条件
24075-48-7
反应条件
1: sodium t-butanolate; biphenyl-2-yl-di-tert-butyl-phosphane; tris-(dibenzylideneacetone)dipalladium(0) / toluene / 24 h / 100 °C / |Inert atmosphere; |Sealed tube 2: Cu(I)[(CH3CN)4]BF4; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; 2,9-dimethyl-1,10-phenanthroline; iodine; methyloxirane / tetrahydrofuran / 20 h / 20 °C / |Flow reactor; |Inert atmosphere; |Irradiation View Scheme
参考文献
Hernandez-Perez, Augusto C.; Collins, Shawn K.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 48 p. 12696 - 12700
Angew. Chem., 2013 , vol. 125, # 48 p. 12928 - 12932
624-31-7
4-碘甲苯
+
87-62-7
→
反应条件
24542-61-8
反应条件
caesium carbonate; P(i-BuNCH2)3CMe; palladium diacetate in toluene T=80°C; Buchwald-Hartwig amination reaction;
参考文献
Iowa State University Research Foundation, Inc.
Patent: US7385058 B1, 2008 ;
Location in patent: Page/Page column 31-34; 35-36 ;
110-91-8
+
201230-82-2
+
624-31-7
4-碘甲苯
→
反应条件
13707-23-8
反应条件
potassium carbonate in toluene T=105°C; P=3000.3 Torr; 12 h;
参考文献
Dang, Tuan T.; Zhu, Yinghuai; Ngiam, Joyce S. Y.; Ghosh, Subhash C.; Chen, Anqi; Seayad, Abdul M.
ACS Catalysis, 2013 , vol. 3, # 6 p. 1406 - 1410
110-89-4
+
201230-82-2
+
624-31-7
4-碘甲苯
→
反应条件
13707-23-8
反应条件
potassium carbonate in toluene T=120°C;
参考文献
Dang, Tuan T.; Zhu, Yinghuai; Ghosh, Subhash C.; Chen, Anqi; Chai, Christina L. L.; Seayad, Abdul M.
Chemical Communications, 2012 , vol. 48, # 12 p. 1805 - 1807
624-31-7
4-碘甲苯
+
104216-55-9
→
反应条件
134257-64-0
反应条件
copper T=180°C; 24 h;
参考文献
Stickley, Kurt R.; Blackstock, Silas C.
Tetrahedron Letters, 1995 , vol. 36, # 10 p. 1585 - 1588
624-31-7
4-碘甲苯
+
108-98-5
→
反应条件
13865-48-0
+
3699-01-2
反应条件
dimethyl sulfoxide; potassium hydroxide T=130°C; 24 h; Inert atmosphere;
参考文献
Yuan, Yu; Thome, Isabelle; Kim, Seok Hwan; Chen, Duanteng; Beyer, Astrid; Bonnamour, Julien; Zuidema, Erik; Chang, Sukbok; Bolm, Carsten
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 17 p. 2892 - 2898
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