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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘甲苯
合成路线
（共 1421 条）
201230-82-2
+
624-31-7
4-碘甲苯
→
反应条件
13222-85-0
4-甲基苯甲酸酐
反应条件
1,3-bis-(diphenylphosphino)propane; water; palladium diacetate; triethylamine in N,N-dimethyl-formamide T=20 - 115°C; P=760.051 Torr; 6 h; Inert atmosphereAutoclave;
参考文献
Li, Yang; Xue, Dong; Wang, Chao; Liu, Zhao-Tie; Xiao, Jianliang
Chemical Communications, 2012 , vol. 48, # 9 p. 1320 - 1322
4319-49-7
N-氨基吗啉
+
624-31-7
4-碘甲苯
→
反应条件
351186-41-9
N-吗啉-4-甲基苯磺酰胺
反应条件
tetrafluoroboric acid; K2S2O5; tetrabutylammomium bromide; palladium diacetate; [(t-Bu)3PH]BF4 in 1,4-dioxane T=80°C; 12 h; Reagent/catalystSolventTemperature;
参考文献
Ye, Shengqing; Wu, Jie
Chemical Communications, 2012 , vol. 48, # 80 p. 10037 - 10039
624-31-7
4-碘甲苯
+
36301-60-7
→
反应条件
351186-41-9
N-吗啉-4-甲基苯磺酰胺
反应条件
1,4-diaza-bicyclo[2.2.2]octane; palladium diacetate; [(t-Bu)3PH]BF4 in 1,4-dioxane T=70°C; 16 h; Inert atmosphere;
参考文献
Emmett, Edward J.; Richards-Taylor, Charlotte S.; Nguyen, Bao; Garcia-Rubia, Alfonso; Hayter, Barry R.; Willis, Michael C.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 20 p. 4007 - 4014
98-01-1
糠醛
+
624-31-7
4-碘甲苯
→
反应条件
34035-05-7
5-(4-甲基苯基)-2-糠醛
反应条件
tetrabutylammomium bromide; potassium acetate; tri-cyclo-hexyl-phosphine; palladium dichloride in N,N-dimethyl-formamide T=110°C; 10 h;
参考文献
McClure; Glover; McSorley; Millar; Osterhout; Roschangar
Organic letters, 2001 , vol. 3, # 11 p. 1677 - 1680
624-31-7
4-碘甲苯
→
反应条件
34035-05-7
5-(4-甲基苯基)-2-糠醛
反应条件
bis-triphenylphosphine-palladium(II) chloride in ethylene glycol dimethyl ether T=50°C; Stille reaction; 2 h;
参考文献
Hosoya, Takamitsu; Aoyama, Hiroshi; Ikemoto, Takaaki; Kihara, Yasutaka; Hiramatsu, Toshiyuki; Endo, Makoto; Suzuki, Masaaki
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 5 p. 663 - 673
624-31-7
4-碘甲苯
+
591-51-5
苯基锂
→
反应条件
640-57-3
苯基对甲苯磺酸
+
3112-84-3
反应条件
1: phenyllithium With DABCO-bis(sulfur dioxide) in 1,4-dioxane T=20°C; 2 h; Inert atmosphereSchlenk technique; 2: 1-(iodo)-4-methylbenzene; 9,9-dimethyl-4,5-bis[bis(4-methoxyphenyl)phosphanyl]xanthene With palladium diacetate; caesium carbonate T=85°C; 16 h; Inert atmosphereSchlenk technique;
参考文献
Emmett, Edward J.; Hayter, Barry R.; Willis, Michael C.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 48 p. 12679 - 12683
Angew. Chem., 2013 , vol. 125, # 48 p. 12911 - 12915,5
2680-03-7
N,N-二甲基丙烯酰胺
+
624-31-7
4-碘甲苯
→
反应条件
34909-37-0
反应条件
triethylamine; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II) in acetonitrile T=100°C;
参考文献
Bernini, Roberta; Cacchi, Sandro; De Salve, Ilse; Fabrizi, Giancarlo
Synlett, 2006 , # 18 p. 2947 - 2952
624-31-7
4-碘甲苯
+
637-44-5
→
反应条件
3287-02-3
反应条件
copper(l) iodide; potassium carbonate; triphenylphosphine in dimethyl sulfoxide T=90°C; 24 h; Inert atmosphere;
参考文献
Li, Tingyi; Sun, Peng; Yang, Hailong; Zhu, Yan; Yan, Hong; Lu, Linhua; Mao, Jincheng
Tetrahedron, 2012 , vol. 68, # 32 p. 6413 - 6419
624-31-7
4-碘甲苯
+
2170-06-1
→
反应条件
3287-02-3
反应条件
KOC(O)Ph; triphenylphosphine; copper(l) chloride in 1,3-dimethyl-imidazolidin-2-one T=120°C; Sila-Sonogashira-Hagihara cross-coupling reaction; 12 h; Inert atmosphere;
参考文献
Ihara, Hideki; Ueda, Akinori; Suginome, Michinori
Chemistry Letters, 2011 , vol. 40, # 9 p. 972 - 974
624-31-7
4-碘甲苯
+
536-74-3
→
反应条件
3287-02-3
反应条件
copper(l) iodide; potassium carbonate; NiCl2((PPh3)P)2 in 1,4-dioxane; water Sonogashira-Hagihara reaction; 4 h; Heating;
参考文献
Imura, Yumi; Shimojuh, Naoya; Kawano, Yuhta; Togo, Hideo
Tetrahedron, 2010 , vol. 66, # 19 p. 3421 - 3426
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