1: n-BuX (X = Li or MgBr) With indium(III) chloride in tetrahydrofuran
T=-78 - 20°C;
2: carbon monoxide; 1-(iodo)-4-methylbenzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=70°C; P=1900 Torr; 3 h;
参考文献
Pena, Miguel A.; Perez Sestelo, Jose; Sarandeses, Luis A.
Synthesis, 2003 , # 5 p. 780 - 784
1: PhCCX (X = Li or MgBr) With indium(III) chloride in tetrahydrofuran
T=-78 - 20°C;
2: carbon monoxide; 1-(iodo)-4-methylbenzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=70°C; P=1900 Torr; 3 h;
参考文献
Pena, Miguel A.; Perez Sestelo, Jose; Sarandeses, Luis A.
Synthesis, 2003 , # 5 p. 780 - 784
1: lithium phenylacetylide With indium(III) chloride in tetrahydrofuran; hexane
T=-78 - 20°C;
2: carbon monoxide; 1-(iodo)-4-methylbenzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; hexane
T=60°C; 1.5 h;
参考文献
Lee, Sung Wook; Lee, Kooyeon; Seomoon, Dong; Kim, Sundae; Kim, Hyunseok; Kim, Hyun; Shim, Eunkyong; Lee, Miae; Lee, Seokju; Kim, Misook; Lee, Phil Ho
Journal of Organic Chemistry, 2004 , vol. 69, # 14 p. 4852 - 4855
