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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
62448-61-7
合成路线
（共 6 条）
201230-82-2
+
108-91-8
环己胺
+
501-65-5
二苯基乙炔
→
反应条件
62448-61-7
反应条件
dodecacarbonyltriiron in tetrahydrofuran T=120°C; P=15001.5 Torr; Autoclave;
参考文献
Driller, Katrin Marie; Klein, Holger; Jackstell, Ralf; Beller, Matthias
Angewandte Chemie, International Edition, 2009 , vol. 48, # 33 p. 6041 - 6044
Angewandte Chemie, 2009 , vol. 121, # 33 p. 6157 - 6160
90841-81-9
+
98-80-6
苯硼酸
→
反应条件
62448-61-7
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in ethanol; water; toluene T=90°C; Suzuki-Miyaura cross-coupling; Inert atmosphere;
参考文献
Onimura, Kenjiro; Matsushima, Mieko; Nakamura, Munetoshi; Tominaga, Tatsuya; Yamabuki, Kazuhiro; Oishi, Tsutomu
Journal of Polymer Science, Part A: Polymer Chemistry, 2011 , vol. 49, # 16 p. 3550 - 3558
24564-83-8
4-氧代-4-(环己基氨基)-2-丁烯酸
→
反应条件
62448-61-7
反应条件
1: 1,1,1,3,3,3-hexamethyl-disilazane; benzene 2: bromine; acetic acid 3: bromine; sodium acetate; acetic acid 4: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; water; toluene / 90 °C / Inert atmosphere View Scheme
参考文献
Onimura, Kenjiro; Matsushima, Mieko; Nakamura, Munetoshi; Tominaga, Tatsuya; Yamabuki, Kazuhiro; Oishi, Tsutomu
Journal of Polymer Science, Part A: Polymer Chemistry, 2011 , vol. 49, # 16 p. 3550 - 3558
1228144-40-8
→
反应条件
62448-61-7
反应条件
1: bromine; sodium acetate; acetic acid 2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; water; toluene / 90 °C / Inert atmosphere View Scheme
参考文献
Onimura, Kenjiro; Matsushima, Mieko; Nakamura, Munetoshi; Tominaga, Tatsuya; Yamabuki, Kazuhiro; Oishi, Tsutomu
Journal of Polymer Science, Part A: Polymer Chemistry, 2011 , vol. 49, # 16 p. 3550 - 3558
1631-25-0
N-环己基马来酰亚胺
→
反应条件
62448-61-7
反应条件
1: bromine; acetic acid 2: bromine; sodium acetate; acetic acid 3: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; water; toluene / 90 °C / Inert atmosphere View Scheme
参考文献
Onimura, Kenjiro; Matsushima, Mieko; Nakamura, Munetoshi; Tominaga, Tatsuya; Yamabuki, Kazuhiro; Oishi, Tsutomu
Journal of Polymer Science, Part A: Polymer Chemistry, 2011 , vol. 49, # 16 p. 3550 - 3558
108-91-8
环己胺
→
反应条件
62448-61-7
反应条件
1: ethyl acetate 2: 1,1,1,3,3,3-hexamethyl-disilazane; benzene 3: bromine; acetic acid 4: bromine; sodium acetate; acetic acid 5: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; water; toluene / 90 °C / Inert atmosphere View Scheme
参考文献
Onimura, Kenjiro; Matsushima, Mieko; Nakamura, Munetoshi; Tominaga, Tatsuya; Yamabuki, Kazuhiro; Oishi, Tsutomu
Journal of Polymer Science, Part A: Polymer Chemistry, 2011 , vol. 49, # 16 p. 3550 - 3558
