bis-triphenylphosphine-palladium(II) chloride; carbon dioxide in 1,4-dioxane T=110°C; P=38000 Torr; 40 h; Title compound not separated from byproducts;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 69, # 4 p. 1065 - 1078
sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride in water; benzene T=30°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
1: With indium in N,N-dimethyl-formamide T=60°C; P=15001.5 Torr; 14 h; Autoclave; 2: With hydrogenchloride; water in ethyl acetate; N,N-dimethyl-formamide regioselective reaction;
参考文献
Miao, Bukeyan; Ma, Shengming
Chemical Communications, 2014 , vol. 50, # 25 p. 3285 - 3287
potassium phosphate buffer; lyophilized Zea mays nitrilase ZmNIT2 EC 3.5.5.1 in water T=30°C; pH=7.15; 14 h; Title compound not separated from byproducts;