反-1,3-二苯基-2-丙稀-1-醇合成路线 （共 76 条）
反应条件
bis(η3-allyl-μ-chloropalladium(II)); 1-mesityl-3-methyl-imidazol-2-ylidene silver iodide; water; triphenylphosphine; potassium hydroxide in dichloromethane T=20°C; 16 h; Inert atmosphere;
参考文献
European Journal of Inorganic Chemistry, , # 13 SPEC. ISS. p. 1796 - 1805
反应条件
1: 2,4-dimethyl-3-pentyl α-trimethylsilanylacetate With (1R,2R)-1,2-diphenyl-1,2-dimethoxyethane; lithium diisopropyl amide in toluene T=-20°C; 1 h; 2: trans-1,3-diphenyl-2-propen-1-one in toluene T=-78°C; 0.5 h;
参考文献
Iguchi, Mayu; Doi, Hirohisa; Hata, Seiji; Tomioka, Kiyoshi
Chemical and Pharmaceutical Bulletin, 2004 , vol. 52, # 1 p. 125 - 129
反应条件
sodium tetrahydroborate in methanol T=20°C; 0.333333 h; Inert atmosphere;
参考文献
Green Chemistry, , vol. 14, # 8 p. 2129 - 2132
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Tetrahedron Letters, , vol. 42, # 13 p. 2477 - 2479
反应条件
1: trimethyl phosphate / 1.5 h / 150 °C 2: LiAlH4 / benzene; tetrahydrofuran / 1.) 10 min, room temp., 2.) reflux, 3 h View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 114, # 7/8 p. 369 - 374
反应条件
in tetrahydrofuran T=20°C; Phenylation; Irradiation;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 12 p. 2761 - 2767
反应条件
n-butyllithium 1.) THF, hexane, -78 deg C, 40 min, 2.) THF, -78 deg C then up to room temperature, 30 min; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 30, # 52 p. 7353 - 7356
反应条件
magnesium 1.) Et2O, 2.) Et2O, reflux; Multistep reaction;
参考文献
Tetrahedron, , vol. 55, # 5 p. 1367 - 1376
反应条件
tert.-butyl lithium 1.)THF, pentane, -120 deg C, 1 h 2.) -78 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 22, # 38 p. 3745 - 3748
参考文献
Journal of the American Chemical Society, , vol. 77, p. 590,592
Journal of the American Chemical Society, , vol. 71, p. 305
Journal of the American Chemical Society, , vol. 77, p. 1814,1817
