1-苯基-1,2-乙二醇二乙酸盐合成路线 (共 74 条)
反应条件
sodium hydroxide in methanol T=50°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Iriuchijima; Kojima
Agricultural and Biological Chemistry, 1982 , vol. 46, # 5 p. 1153 - 1157
反应条件
Bacillus subtilis ECU0554 esterase-expressing Escherichia coli BL21 in ethanol T=35°C; pH=7.5; 0.75 h; aq. phosphate buffer; optical yield given as percent eeenantioselective reaction;
参考文献
Tian, Xin; Zheng, Gao-Wei; Li, Chun-Xiu; Wang, Zhi-Long; Xu, Jian-He
Journal of Molecular Catalysis B: Enzymatic, 2011 , vol. 73, # 1-4 p. 80 - 84
反应条件
1: 0.58 g / Candida antarctica lipase B / acetonitrile; methanol / 110 h 2: PPh3; DEAD / tetrahydrofuran 3: Amberlite IRA-401 / methanol / 1 h View Scheme
参考文献
Virsu, Pauliina; Liljeblad, Arto; Kanerva, Anu; Kanerva, Liisa T.
Tetrahedron Asymmetry, 2001 , vol. 12, # 17 p. 2447 - 2455
反应条件
Bacillus subtilis ECU0554 esterase-expressing Escherichia coli BL21 in ethanol T=35°C; pH=7.5; 2 h; aq. phosphate buffer; optical yield given as percent eeenantioselective reaction;
参考文献
Tian, Xin; Zheng, Gao-Wei; Li, Chun-Xiu; Wang, Zhi-Long; Xu, Jian-He
Journal of Molecular Catalysis B: Enzymatic, 2011 , vol. 73, # 1-4 p. 80 - 84
反应条件
sodium hydroxide in methanol T=50°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Iriuchijima; Kojima
Agricultural and Biological Chemistry, 1982 , vol. 46, # 5 p. 1153 - 1157
反应条件
1: Candida antarctica lipase B / acetonitrile; methanol / 110 h 2: Amberlite IRA-401 / methanol / 1 h View Scheme
参考文献
Virsu, Pauliina; Liljeblad, Arto; Kanerva, Anu; Kanerva, Liisa T.
Tetrahedron Asymmetry, 2001 , vol. 12, # 17 p. 2447 - 2455
反应条件
Bacillus subtilis ECU0554 esterase-expressing Escherichia coli BL21 in ethanol T=35°C; pH=7.5; 2 h; aq. phosphate buffer; optical yield given as percent eeenantioselective reaction;
参考文献
Tian, Xin; Zheng, Gao-Wei; Li, Chun-Xiu; Wang, Zhi-Long; Xu, Jian-He
Journal of Molecular Catalysis B: Enzymatic, 2011 , vol. 73, # 1-4 p. 80 - 84
反应条件
Candida antarctica lipase B in methanol; acetonitrile 110 h;
参考文献
Virsu, Pauliina; Liljeblad, Arto; Kanerva, Anu; Kanerva, Liisa T.
Tetrahedron Asymmetry, 2001 , vol. 12, # 17 p. 2447 - 2455
反应条件
In(OSO2CF3)3 in acetonitrile
T=20°C; Acetylation;
参考文献
Ghaffari Khaligh, Nader
RSC Advances, 2013 , vol. 3, # 1 p. 99 - 110
反应条件
poly(4-vinylpyridine) perchlorate in neat (no solvent)
T=20°C; 0.383333 h;
参考文献
Khaligh, Nader Ghaffari
Journal of Molecular Catalysis A: Chemical, 2012 , vol. 363-364, p. 90 - 100