1-苯基-1,2-乙二醇二乙酸盐合成路线 （共 74 条）
反应条件
[bis(acetoxy)iodo]benzene; [Pd(H2O)2(C10H6C7H4N2CH3)2](2+)*2CF3SO3(1-)=[Pd(H2O)2(C10H6C7H4N2CH3)2](CF3SO3)2
T=20°C; 15 h;
参考文献
Wang, Wenfeng; Wang, Feijun; Shi, Min
Organometallics, 2010 , vol. 29, # 4 p. 928 - 933
反应条件
1: acetic anhydride With peracetic acid; dihydrogen peroxide; acetic acid in water
T=0 - 20°C;
2: styrene With palladium diacetate in water
T=0 - 20°C; chemoselective reaction;
参考文献
Park, Chan Pil; Lee, Joo Ho; Yoo, Kyung Soo; Jung, Kyung Woon
Organic Letters, 2010 , vol. 12, # 11 p. 2450 - 2452
反应条件
1: styrene; acetic acid With [bis(acetoxy)iodo]benzene; water; [Pd(dppp)(H2O)2](2+)(OTf(1-))2
T=20°C; 2 h;
2: acetic anhydride T=20°C; Further stages.;
参考文献
Li, Yang; Song, Datong; Dong, Vy M.
Journal of the American Chemical Society, 2008 , vol. 130, # 10 p. 2962 - 2964
反应条件
C22H26ClN3O2Pd
T=25°C; 8 h;
参考文献
UNIVERSITY OF SOUTHERN CALIFORNIA
Patent: US2010/36131 A1, 2010 ;
Location in patent: Page/Page column 7 ;
反应条件
trifluorormethanesulfonic acid in acetic acid
T=20°C; 2 h;
参考文献
Kang, Yan-Biao; Gade, Lutz H.
Journal of the American Chemical Society, 2011 , vol. 133, # 10 p. 3658 - 3667
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Reginato, Gianna; Ricci, Alfredo; Roelens, Stefano; Scapecchi, Serena
Journal of Organic Chemistry, 1990 , vol. 55, # 17 p. 5132 - 5139
反应条件
tributylphosphine in toluene
Heating;
参考文献
Zeynizadeh, Behzad; Sadighnia, Leila
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 9 p. 2644 - 2648
反应条件
iodine; oxygen; H5PV2Mo10O40
T=80°C; P=1520 Torr; 5 h;
参考文献
Branytska, Olena; Neumann, Ronny
Synlett, 2005 , # 16 art. no. G25505ST, p. 2525 - 2527
反应条件
acetic acid; triethylamine
参考文献
Eastman Chemical Company
Patent: US5623086 A1, 1997 ;
反应条件
potassium fluoride on basic alumina in toluene
2 h;
参考文献
Yadav, Veejendra K; Ganesh Babu; Mittal, Manish
Tetrahedron, 2001 , vol. 57, # 32 p. 7047 - 7051
