1-苯基-1,2-乙二醇二乙酸盐合成路线 (共 74 条)
反应条件
boron trifluoride diethyl etherate
T=20°C; 2 h;
参考文献
Zhong, Wenhe; Yang, Jun; Meng, Xiangbao; Li, Zhongjun
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9997 - 10004
反应条件
1: styrene; acetic acid With [bis(acetoxy)iodo]benzene; [Pd(H2O)2(C10H6C7H4N2CH3)2](2+)*2CF3SO3(1-)=[Pd(H2O)2(C10H6C7H4N2CH3)2](CF3SO3)2; water
T=20°C; 6 h;
2: acetic anhydride T=20°C;
参考文献
Wang, Wenfeng; Wang, Feijun; Shi, Min
Organometallics, 2010 , vol. 29, # 4 p. 928 - 933
反应条件
platinum; benzene
Hydrogenation;
参考文献
Dauben; Evans; Meltzer
Journal of the American Chemical Society, 1941 , vol. 63, p. 1883
反应条件
di-isopropylperoxydicarbonate in acetic acid
T=70°C; 2 h; Further byproducts given;
参考文献
Norman, Julie A.; Thomas, C. Barry; Burrow, Michael J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1087 - 1094
反应条件
Y5(OiPr)13O
T=20°C; Acetylation; transesterification; 1.5 h;
参考文献
Lin, Mei-Huey; RajanBabu
Organic Letters, 2000 , vol. 2, # 7 p. 997 - 1000
反应条件
sodium periodate; lithium bromide
T=95°C; Prevost-Woodward reaction; 18 h; Title compound not separated from byproducts;
参考文献
Emmanuvel, Lourdusamy; Ali Shaikh, Tanveer Mahammad; Sudalai, Arumugam
Organic Letters, 2005 , vol. 7, # 22 p. 5071 - 5074
反应条件
1: 46 percent / ethanol
2: 32 percent / sulfuric acid / 24 h / Heating
3: air, sulfuric acid / (C6H5)2Te2 / 72 h / Heating
View Scheme
参考文献
Kambe, Nobuaki; Fujioka, Toyozo; Ogawa, Akiya; Miyoshi, Noritaka; Sonoda, Noboru
Phosphorus and Sulfur and the Related Elements, 1988 , vol. 38, p. 167 - 176
反应条件
1: potassium acetate
2: benzene; platinum / Hydrogenation
View Scheme
参考文献
Dauben; Evans; Meltzer
Journal of the American Chemical Society, 1941 , vol. 63, p. 1883
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran
1 h; Ambient temperature;
参考文献
Paradisi, Mario Paglialunga; Zecchini, Giampiero Pagani; Torrini, Ines
Tetrahedron Letters, 1986 , vol. 27, # 41 p. 5029 - 5032
反应条件
cesium fluoride in acetonitrile
48 h; Ambient temperature;
参考文献
Mukaiyama, Teruaki; Pai, Fong-Chang; Onaka, Makoto; Narasaka, Koichi
Chemistry Letters, 1980 , p. 563 - 566