1-苯基-1,2-乙二醇二乙酸盐合成路线 （共 74 条）
反应条件
copper diacetate; sodium acetate; Manganese (II) acetate in acetic anhydride
T=95 - 97°C; electrolysis; Yield given. Yields of byproduct given;
参考文献
Shundo, Ryushi; Nishiguchi, Ikuzo; Matsubara, Yoshiharu
Chemistry Letters, 1991 , # 1 p. 185 - 188
反应条件
copper diacetate; Manganese (II) acetate; triethylamine in acetic anhydride
T=95 - 97°C; electrolysis; Yield given. Yields of byproduct given;
参考文献
Shundo, Ryushi; Nishiguchi, Ikuzo; Matsubara, Yoshiharu
Chemistry Letters, 1991 , # 1 p. 185 - 188
反应条件
Y5(OiPr)13O
T=20°C; Acetylation; transesterification; 10 h;
参考文献
Lin, Mei-Huey; RajanBabu
Organic Letters, 2000 , vol. 2, # 7 p. 997 - 1000
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran
T=25°C; Mitsunobu reaction; 21 h; Title compound not separated from byproducts;
参考文献
Virsu, Pauliina; Liljeblad, Arto; Kanerva, Anu; Kanerva, Liisa T.
Tetrahedron Asymmetry, 2001 , vol. 12, # 17 p. 2447 - 2455
反应条件
copper(II) bis(trifluoromethanesulfonate) in dichloromethane
T=20°C; 2 h; Product distribution; Further Variations:Reagentsreaction times;
参考文献
Chandra, Kusum L; Saravanan; Singh, Rajesh K; Singh, Vinod K
Tetrahedron, 2002 , vol. 58, # 7 p. 1369 - 1374
反应条件
1: tetrahydrofuran / 0 °C
2: 30percent H2O2, NaHCO3 / tetrahydrofuran; methanol / Heating
3: DMAP, Et3N
View Scheme
参考文献
Tamao, Kohei; Ishida, Neyoshi
Tetrahedron Letters, 1984 , vol. 25, # 38 p. 4245 - 4248
反应条件
in acetic acid
T=70°C; 2 h; Further byproducts given;
参考文献
Norman, Julie A.; Thomas, C. Barry; Burrow, Michael J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1087 - 1094
反应条件
di-isopropylperoxydicarbonate in acetic acid
T=70°C; 2 h; Yield given. Further byproducts given. Title compound not separated from byproducts;
参考文献
Norman, Julie A.; Thomas, C. Barry; Burrow, Michael J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1087 - 1094
反应条件
di-isopropylperoxydicarbonate in acetic acid
T=70°C; 2 h; Yield given. Further byproducts given. Title compound not separated from byproducts;
参考文献
Norman, Julie A.; Thomas, C. Barry; Burrow, Michael J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1087 - 1094
反应条件
sodium t-butanolate in dimethyl sulfoxide
T=20°C; 0.5 h; Overall yield = > 95 percentSpectr.;
参考文献
Liu, Xuyu; Becker, Bernd; Cooper, Matthew A.
Australian Journal of Chemistry, 2014 , vol. 67, # 4 p. 679 - 683
