1-乙炔-1-(三甲基硅氧基)环己烷合成路线 （共 7 条）
参考文献
Tetrahedron Letters, , vol. 26, # 32 p. 3837 - 3840
反应条件
EDNA
T=120 - 130°C; 15 h;
参考文献
Medvedeva; Novokshonov; Mareev; Borisova
Russian Journal of Organic Chemistry, 2003 , vol. 39, # 3 p. 336 - 339
反应条件
chloro-trimethyl-silane in N-methyl-acetamide; hexane
参考文献
American Cyanamid Company
Patent: US4254285 A1, 1981 ;
Title/Abstract Full Text Show Details
American Cyanamid Company
Patent: US4297516 A1, 1981 ;
反应条件
Aliquatreg; 336; potassium carbonate in Petroleum ether
T=60°C; 4 h;
参考文献
Lissel, M.; Weiffen, J
Synthetic Communications, 1981 , vol. 11, # 7 p. 545 - 550
反应条件
1: 2.3 g / tetrahydrofuran / 5 h / Ambient temperature
2: tetrahydrofuran
View Scheme
参考文献
Lopp; Kobzar; Bergmann; Pehk; Valimae; Viigimaa; Lille
European Journal of Medicinal Chemistry, 1992 , vol. 27, # 2 p. 155 - 159
参考文献
Lopp; Kobzar; Bergmann; Pehk; Valimae; Viigimaa; Lille
European Journal of Medicinal Chemistry, 1992 , vol. 27, # 2 p. 155 - 159
反应条件
2: 1) <bis(trifluoroacetoxy)iodo>benzene, 2) silica gel / 1) CHCl3/CH3CN/H2O, 80 deg C, 10 h, 2) ethyl acetate
View Scheme
参考文献
Tamura, Yasumitsu; Yakura, Takayuki; Haruta, Jun-ichi; Kita, Yasuyuki
Tetrahedron Letters, 1985 , vol. 26, # 32 p. 3837 - 3840
