sodium perchlorate; copper diacetate; sodium acetate; palladium diacetate in acetonitrile T=60°C; electrolysis; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Hartstock, Frederick W.; Wayner, Danial, D. M.
Tetrahedron Letters, 1994 , vol. 35, # 44 p. 8137 - 8140
hydrogenchloride; water in decalin T=225°C; 49 h; in sealed tube; also with DCl/D2O, deuteration investigated; also at 175 deg C; Product distributionMechanism;
参考文献
Werstiuk, Nick Henry; Timmins, George
Canadian Journal of Chemistry, 1985 , vol. 63, p. 530 - 533
in gas byproducts: H2; total static pressure ca. 2E-7 Torr; Fourier transform mass spectrometry; branching ratio NbFe(C7H8)(1+)/Nb(C7H8)(1+) 31/69;
参考文献
Bruckner, Steven W.; Freiser, Ben S.
Journal of Physical Chemistry, 1989 , vol. 93, # 9 p. 3667 - 3673
→
反应条件
in gas byproducts: H2; total static pressure ca. 2E-7 Torr; Fourier transform mass spectrometry; branching ratio NbFe(tropylium)2(1+)/Nb(tol)2(1+) 31/69;
参考文献
Bruckner, Steven W.; Freiser, Ben S.
Journal of Physical Chemistry, 1989 , vol. 93, # 9 p. 3667 - 3673
