3-乙基-1-戊炔-3-醇合成路线 （共 26 条）
参考文献
DE289800 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 12, p. 55
Bulletin de la Societe Chimique de France, , vol. <4>35, p. 604
参考文献
Zhurnal Obshchei Khimii, vol. 10, p. 455
Chem. Zentralbl., , vol. 111, # II p. 1567
Izv. armjansk. Akad.Chem.Abstr., 1941 Nr. 5/6 (10/11) S. 121 , p. 3395
参考文献
Bulletin de la Societe Chimique de France, , vol. <4>35, p. 604
反应条件
hydrogen bromide; copper; copper(I) bromide T=40°C; 1.5 h;
参考文献
Maerkl, G.; Bauer, W.
Tetrahedron Letters, 1993 , vol. 34, # 18 p. 2915 - 2918
反应条件
1: 73 percent / calcium chloride, Cu2Cl2 (95percent brown powder), copper bronze powder, conc. HCl / 1 h / 0 - 5 °C 2: 73 percent / sodium, liq.ammonia / FeCl3 / diethyl ether / overnight View Scheme
参考文献
Kopka, Ihor E.; Fataftah, Zacharia A.; Rathke, Michael W.
Journal of Organic Chemistry, 1980 , vol. 45, # 23 p. 4616 - 4622
反应条件
1: petroleum ether; palladium/barium carbonate / Hydrogenation 2: phosphorus (III)-bromide View Scheme
参考文献
Allais; Mathieu
Annales Pharmaceutiques Francaises, 1951 , vol. 9, p. 275,281
参考文献
Cacace; Zifferero
Ricerca Scientifica, 1956 , vol. 26, p. 1525
反应条件
1: aq. HCl, CaCl2 / CuCl, Cu 2: nBu3SnH, AIBN View Scheme
参考文献
Fantazier,R.M.; Poutsma,M.L.
Journal of the American Chemical Society, 1968 , vol. 90, p. 5490 - 5498
参考文献
Thompson; Burr; Shaw
Journal of the American Chemical Society, 1941 , vol. 63, p. 187
反应条件
1: 73 percent / calcium chloride, Cu2Cl2 (95percent brown powder), copper bronze powder, conc. HCl / 1 h / 0 - 5 °C 2: 48 percent / copper bronze powder, Cu2Cl2, / dimethylformamide / 72 h / 4 °C 3: H2 / 10percent Pd/C / petroleum ether / 10 h / 2585.7 Torr 4: H2 / 10 percent palladium on charcoal / petroleum ether; ethanol 5: BF3 gas / 1 h / 25 °C View Scheme
参考文献
Kopka, Ihor E.; Fataftah, Zacharia A.; Rathke, Michael W.
Journal of Organic Chemistry, 1980 , vol. 45, # 23 p. 4616 - 4622
