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in ethanol T=40°C;

1: 85 percent / iodine / 24 h / Heating View Scheme

in ethanol; water soln. of Co salt in H2O heated to 60-70°C; soln. of ligand in EtOH added over 30 min; stirred at 60-70°C for 2 h; evapd. by 2/3 of initial vol.; cooled to room temp.; stored for 2 d; ppt. collected by filtration; detd. by elem. anal., gravimetric analysis and X-ray diffraction;

in ethanol; water soln. of Ni salt in H2O heated to 60-70°C; soln. of ligand in EtOH added over 30 min; stirred at 60-70°C for 2 h; evapd. by 2/3 of initial vol.; cooled to room temp.; stored for 2 d; ppt. collected by filtration; detd. by elem. anal., gravimetric analysis and X-ray diffraction;

in ethanol Schiff base and metal acetate (2:1 mole ratio) refluxed together in ethanolic medium for 30 min; cryst. ppt. washed (ethanol), dried (vac.), elem. anal.;