反应条件
1: 1.) n-BuLi / 1) THF, hexane, 0.5 h; 2) THF, hexane, 30 deg C, 2 h 2: 0.666 g / aq. HCl / diethyl ether / 0.17 h 3: 95 percent / NaBH4 / methanol 4: triethylamine / CH2Cl2 / 1) 0 deg C, 0.5 h; 2) 30 deg C, 4 h 5: 96 percent / LAH / diethyl ether / 1) 0 deg C, 0.5 h; 2) 30 deg C, 1 h View Scheme
参考文献
Kelkar, S. V.; Joshi, G. S.; Reddy, G. Bhaskar; Kulkarni, G. H.
Synthetic Communications, 1989 , vol. 19, # 7,8 p. 1369 - 1380
