1: 88 percent / ethanol / Heating; E. Wilson and M. Tishler, J. Am. Chem. Soc., 73, 3635 (1951) 2: thionyl chloride / CHCl3 / E. Wilson and M. Tishler, J. Am. Chem. Soc., 73, 3635 (1951) View Scheme
参考文献
Molecular Crystals and Liquid Crystals (1969-1991), , vol. 185, p. 131 - 140
1: 2-mercaptobenzothiazole With sodium hydride in tetrahydrofuran; mineral oil T=0°C; 0.5 h; Inert atmosphere; 2: 1-n-heptylbromide in tetrahydrofuran; mineral oil T=0 - 20°C; Inert atmosphere;
参考文献
Pospiil, Jii; Robiette, Raphael; Sato, Hitoshi; Debrus, Kevin
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 6 p. 1225 - 1234