反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 0.17 h / 0 °C 1.2: hexamethylphosphoric triamide (HMPA) / tetrahydrofuran; hexane / 22 h / 20 °C 2.1: 47.7 g / D-10-camphorsulfonic acid / methanol / 24 h / 20 °C 3.1: H2 / Lindlar's catalyst / hexane / 9 h / 20 °C 4.1: 8.7 g / (COCl)2; DMSO; Et3N / CH2Cl2 / 1 h / 0 °C 5.1: 96 percent / NaClO2; 2-methyl-2-butene; aq. NaH2PO4 / 2-methyl-propan-2-ol / 3 h / 20 °C View Scheme
参考文献
Nakamura, Tsuyoshi; Watanabe, Yukiko; Shiozaki, Masao; Kanai, Saori; Kurakata, Shin-ichi
Bulletin of the Chemical Society of Japan, 2003 , vol. 76, # 5 p. 1011 - 1022
