反应条件
1.1: 96 percent / AgNO3; pyridine / tetrahydrofuran / 12 h 2.1: 92 percent / (COCl)2; DMSO; Et3N / CH2Cl2 / 2 h / -78 - -20 °C 3.1: LiN(SiMe3)2; HMPA / tetrahydrofuran / 1 h / -40 °C 3.2: tetrahydrofuran; hexamethylphosphoric acid triamide / 1.5 h / -78 °C 3.3: 73 percent / methanol; diethyl ether / 0.5 h / 0 °C 4.1: n-Bu4NF / tetrahydrofuran / 3 h / 20 °C 5.1: 90 percent / aq. NaOH / tetrahydrofuran / 20 °C View Scheme
参考文献
Yu, Ming; Alonso-Galicia, Magdalena; Sun, Cheng-Wen; Roman, Richard J.; Ono, Naoya; Hirano, Hitomi; Ishimoto, Tsuyoshi; Reddy, Y. Krishna; Katipally, Kishta Reddy; Reddy, Komandla Malla; Gopal, V. Raj; et al.
Bioorganic & Medicinal Chemistry, 2003 , vol. 11, # 13 p. 2802 - 2822
