2'-甲氧基对甲苯磺酰苯胺合成路线 (共 7 条)
反应条件
in acetonitrile 4 h; Irradiation;
参考文献
Tetrahedron, , vol. 59, # 39 p. 7651 - 7659
反应条件
1: water; nitric acid 2: sulfuric acid View Scheme
参考文献
Bosma; Meerburg; Verkade
Recueil des Travaux Chimiques des Pays-Bas, 1948 , vol. 67, p. 235,238,239
反应条件
in water
T=20°C; 0.5 h;
参考文献
Kamal, Ahmed; Reddy, J. Surendranadha; Bharathi, E. Vijaya; Dastagiri
Tetrahedron Letters, 2008 , vol. 49, # 2 p. 348 - 353
反应条件
copper(l) chloride in methanol
T=20°C; Chan-Lam Coupling; 1 h;
参考文献
Moon, Soo-Yeon; Nam, Jungsoo; Rathwell, Kris; Kim, Won-Suk
Organic Letters, 2014 , vol. 16, # 2 p. 338 - 341
反应条件
potassium phosphate; copper(l) iodide; N-methyl-glycine in N,N-dimethyl-formamide
T=100°C; 24 h;
参考文献
Deng, Wei; Liu, Lei; Zhang, Chen; Liu, Min; Guo, Qing-Xiang
Tetrahedron Letters, 2005 , vol. 46, # 43 p. 7295 - 7298
反应条件
potassium hydroxide in methanol
48 h; Ambient temperature;
参考文献
Sangwan, Naresh K.; Kelkar, Prabhakar M.; Rastogi, Shri Nivas; Anand, N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 639 - 644
反应条件
1: 98 percent / AcOH / benzene / 24 h / Heating
2: 88 percent / pyridine / benzene / 48 h / Ambient temperature
3: 2.1 g / 6N KOH / methanol / 48 h / Ambient temperature
View Scheme
参考文献
Sangwan, Naresh K.; Kelkar, Prabhakar M.; Rastogi, Shri Nivas; Anand, N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 639 - 644