反应条件
1.1: potassium carbonate; potassium hydroxide / water / 5 h / |Reflux 2.1: sodium amide / acetonitrile; tert-butyl methyl ether / 2 h / 0 - 5 °C / |Large scale 2.2: 2 h / 25 °C / |Large scale 3.1: sodium tetrahydroborate; acetic acid / tetrahydrofuran / 3.5 h / 20 °C 3.2: 4 h / 20 °C 3.3: 0.5 h / 20 °C View Scheme
参考文献
Haight, Anthony R.; Stuk, Timothy L.; Allen, Michael S.; Bhagavatula, Lakshmi; Fitzgerald, Michael; Hannick, Steven M.; Kerdesky, Francis A.J.; Menzia, Jerome A.; Parekh, Shyamal I.; Robbins, Timothy A.; Scarpetti, David; Tien, Jien-Heh J.
Organic Process Research and Development, 1999 , vol. 3, # 2 p. 94 - 100
