(i) Mg, Et2O, (ii) (dehydration), (iii) (hydrogenation); Multistep reaction;
参考文献
Cerfontain,H.; Schaasberg-Nienhuis,Z.R.H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1974 , p. 536 - 542
(S)-AlMe(OC6H(CH3)2(C6H4CH3)2)2 in diethyl ether; dichloromethane
T=-78°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;