1,1,1,2-四氯乙烷合成路线 (共 157 条)
反应条件
in n-heptane byproducts: vinyl chloride, 1,1-dichloroethylene, cis-1,2-dichloroethylene; N2-atmosphere; prolonged refluxing; distn., gas chromy. of org. products, IR spectroscopy; further byproducts: trans-1,2-dichloroethylene, 1,1,2-trichloroethane, 1-, 2-, 3-, 4-chloroheptane. CO;
参考文献
Eady, Colin R.; Johnson, Brian F. G.; Lewis, Jack
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1976 , p. 1706 - 1712
反应条件
durch azeotrope Destillation;
参考文献
Weiss
Patent: US2462444 , 1948 ;
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Mason
Journal of the Chemical Society, 1930 , p. 700
参考文献
Steiner
Monatshefte fuer Chemie, 1915 , vol. 36, p. 828
反应条件
hydrogen fluoride; Catalyst M-Chromium oxide T=399.85°C; Fluorination; Product distribution;
参考文献
Kemnitz; Niedersen; Kohne
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1997 , vol. 36, # 6 p. 485 - 493
参考文献
Blicke; Weinkauff
Journal of the American Chemical Society, 1932 , vol. 54, p. 330,333 Anm.9
Journal of the American Chemical Society, 1932 , vol. 54, p. 1460,1462
反应条件
T=75°C; Behandeln des Reaktionsgemisches mit wss. HCl;
参考文献
Hinkel; Ayling; Beynon
Journal of the Chemical Society, 1936 , p. 339,342
参考文献
Hinkel; Ayling; Beynon
Journal of the Chemical Society, 1936 , p. 339,342
反应条件
antimony(V) pentachloride; SbF3 unter Druck;
参考文献
Whalley
Journal of the Society of Chemical Industry, London, 1947 , vol. 66, p. 429
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Henne; Hubbard
Journal of the American Chemical Society, 1936 , vol. 58, p. 404
反应条件
hydrogen fluoride T=225°C; unter Druck;
参考文献
Henne; Hubbard
Journal of the American Chemical Society, 1936 , vol. 58, p. 404
反应条件
fluorinated Fe3O4 2 h; Ambient temperature; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Thomson, James
Journal of the Chemical Society, Faraday Transactions, 1994 , vol. 90, # 23 p. 3585 - 3590