13H-二苯并[a,g]芴-13-酮合成路线 (共 7 条)
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in acetic acid
Heating;
参考文献
Harvey, Ronald G.; Pataki, John; Cortez, Cecilia; Raddo, Pasquale Di; Yang, ChengXi
Journal of Organic Chemistry, 1991 , vol. 56, # 3 p. 1210 - 1217
反应条件
iodine in triglyme (triethylene glycol dimethyl ether)
T=130°C; 0.133333 h; microwave irradiation;
参考文献
Mukhopadhyay; Becker; Banik
Journal of Chemical Research - Part S, 2001 , # 1 p. 28 - 31
参考文献
Fuson; Wassmundt
Journal of the American Chemical Society, 1956 , vol. 78, p. 5409,5411
反应条件
NaBiO3
T=20°C; Acetoxylation; 16 h;
参考文献
Banik, Bimal K.; Ghatak, Anjan; Mukhopadhyay, Chhanda; Becker, Frederick F.
Journal of Chemical Research - Part S, 2000 , # 3 p. 108 - 109
反应条件
chromic acid; lithium diisopropyl amide
2) THF, rt; Yield given. Multistep reaction;
参考文献
Fu, Jian-min; Zhao, Bao-ping; Sharp, M. J.; Snieckus, V.
Journal of Organic Chemistry, 1991 , vol. 56, # 5 p. 1683 - 1685
反应条件
1: AlCl3; nitrobenzene
2: copper-powder; quinoline
View Scheme
参考文献
Campbell
Journal of the Chemical Society, 1954 , p. 3659,3668
反应条件
dipotassium peroxodisulfate; palladium; trifluoroacetic acid
20.3 h; Inert atmosphere;
参考文献
Elman, Alexander R.
Tetrahedron Letters, 2013 , vol. 54, # 40 p. 5527 - 5531