(E)-1-甲氧基-2-(2-硝基-1-丙烯基)苯合成路线 （共 9 条）
反应条件
hydrogenchloride; iron(III) chloride; iron 1 h; Heating;
参考文献
Binovic,K.; Vrancea,S.
Chimica Therapeutica, 1968 , vol. 3, p. 313 - 320
反应条件
lithium aluminium tetrahydride
参考文献
Bailey,K. et al.
Canadian Journal of Chemistry, 1971 , vol. 49, p. 3143 - 3151
反应条件
ammonium acetate
Henry condensation; Reflux;
参考文献
Backstroma, Nicholas; Burtona, Neil A.; Watta, C. Ian F.
Journal of Physical Organic Chemistry, 2010 , vol. 23, # 8 p. 711 - 722
参考文献
Schmidt,E. et al.
Chemische Berichte, 1922 , vol. 55, p. 1756
参考文献
Schmidt; Baejen
Patent: DE348382 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 1416
Full Text Show Details
Schmidt,E. et al.
Chemische Berichte, 1922 , vol. 55, p. 1756
反应条件
hydrogenchloride; potassium hydroxide
1) ether, reflux, 2) methanol, water, 0.5 h, reflux; Yield given. Multistep reaction;
参考文献
Boberg, Friedrich; Garburg, Karl-Heinz; Goerlich, Karl-Joachim; Pipereit, Eberhard; Ruhr, Maria
Liebigs Annalen der Chemie, 1985 , # 2 p. 239 - 250
反应条件
1: sodium tetrahydroborate; sodium hydroxide / ethanol / 1 h / 0 °C
2: boron tribromide / chloroform / -78 - 20 °C / Inert atmosphere
3: sodium hydroxide / methanol; water / 0.08 h
View Scheme
参考文献
Backstroma, Nicholas; Burtona, Neil A.; Watta, C. Ian F.
Journal of Physical Organic Chemistry, 2010 , vol. 23, # 8 p. 711 - 722
参考文献
Boberg, Friedrich; Garburg, Karl-Heinz; Goerlich, Karl-Joachim; Pipereit, Eberhard; Redelfs, Elke; Ruhr, Maria
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 1853 - 1859
反应条件
hydrogenchloride; potassium hydroxide
1) ether, reflux, 2) methanol, water, 0.5 h, reflux; Yield given. Multistep reaction;
参考文献
Boberg, Friedrich; Garburg, Karl-Heinz; Goerlich, Karl-Joachim; Pipereit, Eberhard; Ruhr, Maria
Liebigs Annalen der Chemie, 1985 , # 2 p. 239 - 250
