4-硝基-N-甲基-苯磺酰胺合成路线 (共 13 条)
反应条件
in diethyl ether; water 16 h; Ambient temperature;
参考文献
Khanna, Ish K.; Weier, Richard M.; Yu, Yi; Collins, Paul W.; Miyashiro, Julie M.; Koboldt, Carol M.; Veenhuizen, Amy W.; Currie, Jerry L.; Seibert, Karen; Isakson, Peter C.
Journal of Medicinal Chemistry, 1997 , vol. 40, # 11 p. 1619 - 1633
反应条件
methylamine in dichloromethane
参考文献
G. D. Searle and Co.
Patent: US5932598 A1, 1999 ;
反应条件
1: With 1-methyl-pyrrolidin-2-one T=50°C; 0.25 h; 2: With ammonia in methanol T=20°C; 0.0833333 h;
参考文献
Journal of the American Chemical Society, , vol. 125, # 34 p. 10168 - 10169
反应条件
pyridine; 2-(N,N-dimethylamino)-pyridine; ammonia; N-ethyl-N,N-diisopropylamine; methyl iodide in methanol
参考文献
MacLean, Derek; Star-Lack, Joshua M.
Patent: US2004/131544 A1, 2004 ;
反应条件
silver benzoate in 1,4-dioxane; water T=70°C; 5 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 13 p. 4798 - 4802
反应条件
dichloro-acetic acid in water-d2 other acids; acid-catalysed denitrosation of substituted N-methyl-N-nitrosobenzenesulfonamides; reversibility; kinetics of nitrosation and denitrosation; general-acid catalysis; effect of nucleophiles; kinetic solvent isotope effect; mechanism; Rate constantEquilibrium constant;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 7 p. 1613 - 1620
反应条件
sulfuric acid in water T=25°C; Dependence of the decomposition rate on concentration of H2SO4; Rate constant;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, # 4 p. 671 - 675
Zhurnal Organicheskoi Khimii, , vol. 19, # 4 p. 761 - 766
反应条件
in 1,4-dioxane; water T=25°C; Rate constant;
参考文献
Journal of Physical Organic Chemistry, , vol. 11, # 10 p. 756 - 760
反应条件
hydrogen; nickel in methanol T=25°C; P=258.6 Torr; 20 h;
参考文献
Khanna, Ish K.; Weier, Richard M.; Yu, Yi; Collins, Paul W.; Miyashiro, Julie M.; Koboldt, Carol M.; Veenhuizen, Amy W.; Currie, Jerry L.; Seibert, Karen; Isakson, Peter C.
Journal of Medicinal Chemistry, 1997 , vol. 40, # 11 p. 1619 - 1633
参考文献
G. D. Searle and Co.
Patent: US5932598 A1, 1999 ;