1,1,2,2-四苯基乙烷合成路线 (共 396 条)
反应条件
aluminium trichloride
参考文献
Biltz
Chemische Berichte, 1893 , vol. 26, p. 1952
Justus Liebigs Annalen der Chemie, 1897 , vol. 296, p. 219
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Combes
Annales de Chimie (Cachan, France), 1887 , vol. <6> 12, p. 263
Bulletin de la Societe Chimique de France, 1894 , vol. <3> 11, p. 710
参考文献
Stadnikow
Chemische Berichte, 1924 , vol. 57, p. 1
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Sabatier; Murat
Annales de Chimie (Cachan, France), 1915 , vol. <9> 4, p. 279
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Stadnikow
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1916 , vol. 48, p. 1871
Chemische Berichte, 1924 , vol. 57, p. 7
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Sabatier; Murat
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1913 , vol. 157, p. 1497
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1914 , vol. 158, p. 535
反应条件
sodium peroxodisulphate; sulfuric acid; silver nitrate; copper(II) sulfate
1.) water, reflux, 2.) 5 min, reflux; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Fristad, William E.; Fry, Melisa A.; Klang, Jeffrey A.
Journal of Organic Chemistry, 1983 , vol. 48, # 20 p. 3575 - 3577
反应条件
zinc
2 h; Heating; Further byproducts given;
参考文献
Vona, Maria Luisa Di; Rosnati, Vittorio
Journal of Organic Chemistry, 1991 , vol. 56, # 13 p. 4269 - 4273
反应条件
in benzene
Heating; Further byproducts given;
参考文献
Benati, Luisa; Montevecchi, P. Carlo; Spagnolo, Piero
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 917 - 922
反应条件
n-butyllithium
1.) diethyl ether, hexane, 2 h, 2.) diethyl ether, hexane, 16 h; Multistep reaction;
参考文献
Eisch, John J.; Kovacs, Csaba A.; Chobe, Prabodh; Boleslawski, Marek P.
Journal of Organic Chemistry, 1987 , vol. 52, # 20 p. 4427 - 4437
反应条件
n-butyllithium
1.) diethyl ether, hexane, 90 min, 2.) diethyl ether, hexane; Yield given. Multistep reaction;
参考文献
Eisch, John J.; Kovacs, Csaba A.; Chobe, Prabodh; Boleslawski, Marek P.
Journal of Organic Chemistry, 1987 , vol. 52, # 20 p. 4427 - 4437
反应条件
1: CH2Cl2 / Ambient temperature
2: 69 percent / tetrahydrofuran / 1 h / -64 °C / Irradiation
View Scheme
参考文献
Barton, Derek H. R.; Bridon, Dominique; Fernandez-Picot, Isabel; Zard, Samir Z.
Tetrahedron, 1987 , vol. 43, # 12 p. 2733 - 2740
反应条件
2,4,6-triphenylpyrylium-tetrafluoroborate in acetonitrile
IrradiationInert atmosphere;
参考文献
Bonesi, Sergio M.; Fagnoni, Maurizio; Albini, Angelo
European Journal of Organic Chemistry, 2008 , # 15 p. 2612 - 2620
参考文献
Schlenk; Bergmann
Justus Liebigs Annalen der Chemie, 1928 , vol. 463, p. 208
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Bergmann
Chemische Berichte, 1930 , vol. 63, p. 1626
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Kliegl
Chemische Berichte, 1929 , vol. 62, p. 1330
Chemische Berichte, 1931 , vol. 64, p. 2422