1,1,2,2-四苯基乙烷合成路线 (共 396 条)
反应条件
ytterbium; methyl iodide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide
2 h; Ambient temperature;
参考文献
Makioka, Yoshikazu; Uebori, Shin-Ya; Tsuno, Masumi; Taniguchi, Yuki; Takaki, Ken; Fujiwara, Yuzo
Journal of Organic Chemistry, 1996 , vol. 61, # 1 p. 372 - 375
反应条件
hydrogenchloride; acetic acid; zinc
T=10°C; 1 h; Further byproducts given;
参考文献
Vona, Maria Luisa Di; Rosnati, Vittorio
Journal of Organic Chemistry, 1991 , vol. 56, # 13 p. 4269 - 4273
反应条件
water in chlorobenzene
Ambient temperature;
参考文献
Barton, Derek H. R.; Bridon, Dominique; Zard, Samir Z.
Tetrahedron Letters, 1986 , vol. 27, # 36 p. 4309 - 4312
反应条件
mercury; zinc
T=25°C; 1 h;
参考文献
Vona, Maria Luisa Di; Rosnati, Vittorio
Journal of Organic Chemistry, 1991 , vol. 56, # 13 p. 4269 - 4273
反应条件
pentacarbonyliron
T=140°C; 48 h;
参考文献
Luh, Tien-Yau; Lee, Kim Sze; Tam, S. W.
Journal of Organometallic Chemistry, 1981 , vol. 219, # 3 p. 345 - 352
反应条件
copper in toluene
2 h; Heating;
参考文献
West; Naidu
Journal of Organic Chemistry, 1994 , vol. 59, # 20 p. 6051 - 6056
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
0.583333 h;
参考文献
Singh, P. R.; Khurana, J. M.; Nigam, Alok
Tetrahedron Letters, 1981 , vol. 22, # 30 p. 2901 - 2904
反应条件
1: 1,1-diphenyl-2-propanone With potassium tert-butylate in tetrahydrofuran
T=0°C; 2 h;
2: 1-chloro-1,1-diphenylmethane in tetrahydrofuran
2 h; Heating;
参考文献
Zieger, Herman E.; Tsang, Choi Han; Malik, Mohammed; Todaro, Louis J.
Tetrahedron Letters, 2002 , vol. 43, # 27 p. 4845 - 4848
反应条件
1: platinum; acetic acid / Hydrogenation
2: benzene; HgO / 10 °C
3: 114 °C
View Scheme
参考文献
Cohen; Wang
Journal of the American Chemical Society, 1955 , vol. 77, p. 2457,2460
反应条件
2-chloro-5-carboxybenzene in tetrahydrofuran
T=0 - 20°C; Inert atmosphere;
参考文献
Azzena, Ugo; Dettori, Giovanna; Mocci, Sarah; Pisano, Luisa; Cerioni, Giovanni; Mocci, Francesca
Tetrahedron, 2010 , vol. 66, # 47 p. 9171 - 9174