2,3-二甲氧基-5-硝基-苯甲醛合成路线 (共 10 条)
反应条件
boron tribromide in dichloromethane T=-78°C; regioselective reaction;
参考文献
Groszek, Grazyna; Bajek, Agata; Bis, Agnieszka; Nowak-Krol, Agnieszka; Bednarski, Marek; Siwek, Agata; Filipek, Barbara
Molecules, 2010 , vol. 15, # 6 p. 3887 - 3904
参考文献
Davies
Journal of the Chemical Society, 1923 , vol. 123, p. 1584
反应条件
nitric acid in acetic acid
0.75 h; Ambient temperature;
参考文献
Fukuyama, Yoshiyasu; Iwatsuki, Chie; Kodama, Mitsuaki; Ochi, Masamitsu; Kataoka, Kumi; Shibata, Kozo
Tetrahedron, 1998 , vol. 54, # 34 p. 10007 - 10016
反应条件
potassium carbonate in water; acetone
Heating;
参考文献
Maguet,M. et al.
Bulletin de la Societe Chimique de France, 1978 , vol. <II>, p. 550 - 560
反应条件
hydrogenchloride; acetic acid
参考文献
Murakami
Justus Liebigs Annalen der Chemie, 1932 , vol. 496, p. 125,140
Proceedings of the Imperial Academy (Tokyo), vol. 7, p. 256
Chem. Zentralbl., 1931 , vol. 102, # II p. 2623
反应条件
chloroform; silver(l) oxide
参考文献
Davies
Journal of the Chemical Society, 1923 , vol. 123, p. 1584
参考文献
Perkin; Robinson
Journal of the Chemical Society, 1914 , vol. 105, p. 2384
Full Text Show Details
Perkin; Robinson; Stoyle
Journal of the Chemical Society, 1924 , vol. 125, p. 1357
参考文献
Davies
Journal of the Chemical Society, 1923 , vol. 123, p. 1584
参考文献
Davies
Journal of the Chemical Society, 1923 , vol. 123, p. 1584
反应条件
sodium hydrogensulfite; iron(II) sulfate; calcium carbonate
Reagens 4:Wasser;Behandeln der filtrierten Reaktionsloesung mit wss.HCl und mit wss.NaNO2 bei 3grad und Erwaermen der erhaltenen Diazoniumsalz-Loesung;
参考文献
Smith; La Forge
Journal of the American Chemical Society, 1931 , vol. 53, p. 3072,3076