1-二乙氧基磷酰-1-硝基-丙烷合成路线 (共 3 条)
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
T=20°C; 72 h;
参考文献
Bera, Kalisankar; Namboothiri, Irishi N. N.
Organic Letters, 2012 , vol. 14, # 4 p. 980 - 983
参考文献
Fujii, Masayuki
Chemistry Letters, 1992 , # 6 p. 933 - 934
反应条件
lithium diisopropyl amide
1.) THF, -78 deg C, 0.5 h, 2.) -78 deg C, 3 h; -30 deg C, 2h; Yield given. Multistep reaction;
参考文献
Kandil, Ali A.; Porter, Terence M.; Slessor, Keith N.
Synthesis, 1987 , # 4 p. 411 - 413