2-氰基-N-甲基乙酰胺合成路线 （共 18 条）
反应条件
sodium hydride
1) THF, room temperature, 2) room temperature; Yield given. Multistep reaction;
参考文献
Yokoyama, Masataka; Kodera, Masahito; Imamoto, Tsuneo
Journal of Organic Chemistry, 1984 , vol. 49, p. 74 - 78
反应条件
sodium hydride
1) THF, room temperature, 2) room temperature; Yield given. Multistep reaction;
参考文献
Yokoyama, Masataka; Kodera, Masahito; Imamoto, Tsuneo
Journal of Organic Chemistry, 1984 , vol. 49, p. 74 - 78
反应条件
acetic acid; sodium nitrite
参考文献
Shaw et al.
Journal of the Chemical Society, 1959 , p. 1648,1652
反应条件
hydrogen sulfide; triethylamine in ethanol
T=70°C; 1.5 h;
参考文献
Morzherin; Kosterina; Berseneva; Dehaen; Bakulev
Russian Chemical Bulletin, 2002 , vol. 51, # 7 p. 1292 - 1297
反应条件
aminosulfonic acid
0.05 h; microwave irradiation;
参考文献
Reddy, Y. Thirupathi; Reddy, P. Raghotham; Reddy, M. Nikhil; Rajitha; Crooks, Peter A.
Synthetic Communications, 2008 , vol. 38, # 18 p. 3201 - 3207
反应条件
sulfur; triethylamine in N,N-dimethyl-formamide
参考文献
Devani; Shishoo; Pathak; Parikh; Radhakrishnan; Padhya
Arzneimittel-Forschung/Drug Research, 1977 , vol. 27, # 9 p. 1652 - 1655
反应条件
sulfur; diethylamine in ethanol
T=20°C; 120 h;
参考文献
N.V. ORGANON
Patent: WO2008/3452 A1, 2008 ;
Location in patent: Page/Page column 68-69 ;
WO 2008/003452 A1
参考文献
Hirota; Kitade; Senda; et al.
Journal of Organic Chemistry, 1981 , vol. 46, # 5 p. 846 - 851
