(2-甲基苄基)三苯基氯化膦合成路线 (共 5 条)
反应条件
in toluene T=110°C; Inert atmosphere;
参考文献
Coulombel, Lydie; Weiwer, Michel; Dunach, Elisabet
European Journal of Organic Chemistry, 2009 , # 33 p. 5788 - 5795
反应条件
T=100°C; 0.166667 h; Inert atmosphereneat (no solvent);
参考文献
Byrne, Peter A.; Gilheany, Declan G.
Journal of the American Chemical Society, 2012 , vol. 134, # 22 p. 9225 - 9239
反应条件
sodium hydroxide in dichloromethane 0.5 h; Ambient temperature;
参考文献
Bookham, Jonathan L.; Smithies, Darren M.; Wright, Anna; Thornton-Pett, Mark; McFarlane, William
Journal of the Chemical Society - Dalton Transactions, 1998 , # 5 p. 811 - 818
反应条件
T=200 - 300°C; 6 h; Inert atmosphere;
参考文献
Dyes and Pigments, , vol. 105, p. 216 - 222
反应条件
1: aq. sodium hydroxide / CH2Cl2 / 0.5 h / Ambient temperature
2: bromine / CCl4 / 0.5 h / 70 °C
3: potassium hydroxide / ethanol / 12 h / Heating
View Scheme
参考文献
Bookham, Jonathan L.; Smithies, Darren M.; Wright, Anna; Thornton-Pett, Mark; McFarlane, William
Journal of the Chemical Society - Dalton Transactions, 1998 , # 5 p. 811 - 818