2,4-二甲基-1,3-苯二酚合成路线 （共 26 条）
参考文献
Journal of the Chemical Society, , p. 2834
Journal of the Chemical Society, , p. 611
Yakugaku Zasshi, , vol. 54, p. 488,490;dtsch.Ref.S.79,82
Chem.Abstr., , p. 97
参考文献
Monatshefte fuer Chemie, , vol. 90, p. 609,619
反应条件
sodium borohydride; boron trifluoride-diethyl ether complex in tetrahydrofuran; water
参考文献
Standard Oil Company (Indiana)
Patent: US4130719 A1, 1978 ;
参考文献
Statens Serum Institute
Patent: US2003/65039 A1, 2003 ;
反应条件
1: BF3*Et2O / 120 °C
2: H2O / tetrahydrofuran / Heating
View Scheme
参考文献
Nicolaou; Vassilikogiannakis, Georgios; Simonsen, Klaus B.; Baran, Phil S.; Zhong, Yong-Li; Vidali, Veroniki P.; Pitsinos, Emmanuel N.; Couladouros, Elias A.
Journal of the American Chemical Society, 2000 , vol. 122, # 13 p. 3071 - 3079
反应条件
hydrogenchloride; diethyl ether; zinc(II) chloride
und Erwaermen des Reaktionsprodukts mit H2O;
参考文献
Kuhn; Staab
Chemische Berichte, 1954 , vol. 87, p. 262,264
反应条件
1: BF3*Et2O / 120 °C
2: H2O / tetrahydrofuran / Heating
View Scheme
参考文献
Kuhn; Staab
Chemische Berichte, 1954 , vol. 87, p. 262,264
反应条件
diethyl ether; boron trifluoride
参考文献
Smith; Thomson
Journal of the Chemical Society, 1960 , p. 346,349
反应条件
ethylmagnesium bromide
1.) diethyl ether, rt; 2.) toluene, rt, 5 h; Yield given. Multistep reaction;
参考文献
Bigi, Franca; Casiraghi, Giovanni; Casnati, Giuseppe; Marchesi, Stefania; Sartori, Giovanni; Vignali, Carlo
Tetrahedron, 1984 , vol. 40, # 20 p. 4081 - 4084
反应条件
1: 41 percent / BF3-etherate / 2.5 h / 100 °C
2: 77 percent / Zn / acetic acid; diethyl ether / 2 h / Ambient temperature
View Scheme
参考文献
Trifonov,L.S.; Bieri,J.H.
Tetrahedron, 1983 , vol. 39, p. 4243
