N-甲基-N-亚硝基苯甲酰胺合成路线 (共 17 条)
反应条件
methanol; ammonium hydroxide in dichloromethane 48 h; Ambient temperature;
参考文献
Garcia, Jordi; Gonzalez, Javier; Segura, Ramon; Urpi, Felix; Vilarrasa, Jaume
Journal of Organic Chemistry, 1984 , vol. 49, # 18 p. 3322 - 3327
反应条件
in dichloromethane T=40°C; 11 h; Product distribution;
参考文献
Garcia, Jordi; Gonzalez, Javier; Segura, Ramon; Urpi, Felix; Vilarrasa, Jaume
Journal of Organic Chemistry, 1984 , vol. 49, # 18 p. 3322 - 3327
反应条件
4 A molecular sieve; sodium hydride THF, 2.) room temp., 20 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Synthesis, , # 4 p. 305 - 306
反应条件
in dichloromethane Heatingweek-end; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 23, # 10 p. 1127 - 1128
反应条件
in dichloromethane T=40°C; 11 h; Yield given;
参考文献
Garcia, Jordi; Gonzalez, Javier; Segura, Ramon; Urpi, Felix; Vilarrasa, Jaume
Journal of Organic Chemistry, 1984 , vol. 49, # 18 p. 3322 - 3327
反应条件
acetic acid; zinc T=10 - 15°C;
参考文献
Garcia, Jordi; Vilarrasa, Jaume
Tetrahedron Letters, 1987 , vol. 28, # 3 p. 341 - 342
反应条件
hydrogenchloride; tin(ll) chloride in diethyl ether Ambient temperature;
参考文献
Garcia, Jordi; Vilarrasa, Jaume
Tetrahedron Letters, 1987 , vol. 28, # 3 p. 341 - 342
反应条件
4 A molecular sieve; sodium hydride THF, 2.) room temp., 20 min; Yield given. Multistep reaction;
参考文献
Berenguer, Ramon; Garcia, Jordi; Vilarrasa, Jaume
Synthesis, 1989 , # 4 p. 305 - 306
反应条件
sodium acetate; nitrogen(IV) oxide in dichloromethane
T=-20°C;
参考文献
Garcia, Jordi; Gonzalez, Javier; Segura, Ramon; Urpi, Felix; Vilarrasa, Jaume
Journal of Organic Chemistry, 1984 , vol. 49, # 18 p. 3322 - 3327
反应条件
silver nitrate in acetonitrile
T=-45°C; 0.5 h; other temperatures; other N-benzylbenzimidoyl chlorides; influence of electron transfer agents, and N,N-dimethyl-4-toluidine; Product distributionMechanism;
参考文献
Iley, Jim; Carvalho, Emilia; Norberto, Fatima; Rosa, Eduarda
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1992 , # 2 p. 281 - 290