反应条件
1: 1,2,3-Benzotriazole; thionyl chloride / dichloromethane / 2.5 h / 25 °C / |Inert atmosphere; |Schlenk technique 2: bis(1,5-cyclooctadiene)nickel (0); diphenylcyclohexyl phosphine; triethylamine; triethylsilyl trifluoromethanesulphonate / toluene / 2 h / 25 °C / 760.05 Torr 3: C40H37ClIrN5; sodium t-butanolate / benzene-d6 / 80 °C / |Inert atmosphere; |Glovebox View Scheme
参考文献
Organometallics, , vol. 33, # 2 p. 473 - 484