N-(4-(4-乙酰氨基-3-硝基苯基)-2-硝基苯基)乙酰胺合成路线 (共 10 条)
反应条件
potassium carbonate; C28H30Cl2N2O4Pd2S4 in toluene T=110°C; Suzuki Coupling; 10 h;
参考文献
WO2005/92839 A1, ;
Page/Page column 5; 7-8 ;
参考文献
Chemische Berichte, , vol. 20, p. 1026
Chemische Berichte, , vol. 5, p. 236
反应条件
1: acetic acid / 0.25 h 2: conc. HNO3 / 100 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 115, # 11 p. 4532 - 4539
反应条件
1: 1.) Hg(OAc)2, AcOH, HClO4, 2.) Cu, PdCl2, pyridine 2: HNO3 / acetic acid View Scheme
参考文献
Chemical Communications, , # 10 p. 929 - 930
反应条件
1: H2SO4 2: H2 / Raney Ni View Scheme
参考文献
Brunner; Witt
Chemische Berichte, 1887 , vol. 20, p. 1026
反应条件
1: aq. H2SO4 / 1 h / 100 °C 2: 1.) sodium nitrite, conc. H2SO4, 2.) glacial acetic acid, CuO / 1.) 10 deg C 1 h, 2.) EtOH, 30 min 3: 59 percent / SnCl2*2H2O / ethanol / 1 h / 70 °C View Scheme
参考文献
Minato, Masaki; Lahti, Paul M.; Van Willigen, Hans
Journal of the American Chemical Society, 1993 , vol. 115, # 11 p. 4532 - 4539
反应条件
potassium hydroxide in ethanol; water 0.666667 h;
参考文献
COUNCIL OF SCIENTIFIC AND INDUSTRIAL RESEARCH
Patent: WO2005/92839 A1, 2005 ;
Location in patent: Page/Page column 8 ;
反应条件
25 prozentige Kalilauge;
参考文献
Hodgson; Gorowara
Journal of the Chemical Society, 1926 , p. 1758
参考文献
Cain; Coulthard; Micklethwait
Journal of the Chemical Society, 1912 , vol. 101, p. 2303
反应条件
1: aq. H2SO4 / 1 h / 100 °C
2: 1.) sodium nitrite, conc. H2SO4, 2.) glacial acetic acid, CuO / 1.) 10 deg C 1 h, 2.) EtOH, 30 min
View Scheme
参考文献
Minato, Masaki; Lahti, Paul M.; Van Willigen, Hans
Journal of the American Chemical Society, 1993 , vol. 115, # 11 p. 4532 - 4539