N-[(3-(苯胺基亚甲基)-2-氯-1-环己烯-1-基)亚甲基]苯胺盐酸盐合成路线 （共 13 条）
反应条件
1: cyclohexanone; N,N-dimethyl-formamide With trichlorophosphate Vilsmeier-Haack Formylation; 1 h; Reflux; 2: aniline in ethanol T=20°C; Vilsmeier-Haack Formylation; 0.5 h;
参考文献
Okoh, Okoh Adeyi; Bisby, Roger H.; Lawrence, Clare L.; Rolph, Carole E.; Smith, Robert B.
Journal of Sulfur Chemistry, 2014 , vol. 35, # 1 p. 42 - 56
反应条件
1: in ethanol T=20°C; 0.5 h; 2: With hydrogenchloride in ethanol; water T=5°C;
参考文献
Kyoto University; Shimadzu Corporation; SAJI, Hideo; KIMURA, Shunsaku; ONO, Masahiro; TEMMA, Takashi; HARA, Isao; OZEKI, Eiichi
Patent: EP2682131 A1, 2014 ;
Location in patent: Paragraph 0140 ;
反应条件
1: With trichlorophosphate in dichloromethane 2: With hydrogenchloride; aniline in ethanol; water T=4°C;
参考文献
EP1221465 A1, ;
Example 18 ;
反应条件
1.1: trichlorophosphate / 0 °C / Reflux 1.2: 1 h / 20 °C 2.1: hydrogenchloride / water View Scheme
参考文献
Chemistry - A European Journal, , vol. 17, # 13 p. 3619 - 3629
反应条件
1.1: trichlorophosphate / 0 °C / Reflux 1.2: 1 h / 20 °C 2.1: hydrogenchloride / water View Scheme
参考文献
Chemistry - A European Journal, , vol. 17, # 13 p. 3619 - 3629
反应条件
sodium acetate in ethanol 1 h; Reflux;
参考文献
EASTMAN KODAK COMPANY; WIDZINSKI, Thomas, J.; PAWLIK, Thomas, D.; OLM, Myra, Toffolon; BOSE, Judith, A.
Patent: WO2013/55640 A2, 2013 ;
Location in patent: Page/Page column 25 ;
反应条件
acetic anhydride T=50°C; 3 h;
参考文献
KODAK POLYCHROME GRAPHICS GMBH
Patent: WO2004/52995 A1, 2004 ;
Location in patent: Page 24 ;
反应条件
1: NaOAc / ethanol / Heating
2: Et3N / ethanol / Heating
View Scheme
参考文献
Slominskii,Yu.L. et al.
Journal of Organic Chemistry USSR (English Translation), 1978 , vol. 14, p. 2046 - 2051
Zhurnal Organicheskoi Khimii, 1978 , vol. 14, p. 2214 - 2221
反应条件
1: NaOAc / ethanol / Heating
2: Et3N / ethanol / Heating
View Scheme
参考文献
Slominskii,Yu.L. et al.
Journal of Organic Chemistry USSR (English Translation), 1978 , vol. 14, p. 2046 - 2051
Zhurnal Organicheskoi Khimii, 1978 , vol. 14, p. 2214 - 2221
反应条件
1: Et3N / ethanol
2: NaOAc / ethanol / Heating
View Scheme
参考文献
Slominskii,Yu.L. et al.
Journal of Organic Chemistry USSR (English Translation), 1978 , vol. 14, p. 2046 - 2051
Zhurnal Organicheskoi Khimii, 1978 , vol. 14, p. 2214 - 2221
