in benzene
byproducts: SnCl(4-FC6H4)3; 25°C; not isolated, reaction followed by NMR spectroscopy;
参考文献
Kravtsov, Dmitrii N.; Peregudov, Alexander S.; Pachevskaya, Valentina M.; Golovchenko, Lyudmila S.
Journal of Organometallic Chemistry, 1997 , vol. 536-537, p. 385 - 388
hydrogenchloride in toluene
byproducts: BrMgCl; n-heptylmagnesium bromide added dropwise at 0°C over 30 min to stoich. amt. of organotin chloride suspended in toluene under inert atm.; mixt. refluxed for 6 h; cooled to room temp.; hydrolyzed with 7percent HCl; org. layer sepd.; dried overnight (anhyd. Na2SO4); filtered; solvent evapd.; purified by vac. distn.; elem. anal.;
参考文献
Sadiq-ur-Rehman; Ali, Saqib; Badshah, Amin
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 2004 , vol. 34, # 3 p. 443 - 457
